GCMS analysis results, sample AD29135, Dec 2001

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Laboratory report showing GCMS scan results for sample AD29135 including detection of unknown compounds and surrogates.

NYC-WTC_000036079–000036091

Folder label: “GCMS X 12/3/01 A 12/10/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC1001\29234.D Vial: 23 Acq On : 11 Dec 2001 8:10 am Operator: 209 GALOS Sanpl e : gc/ms scan 12/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.33 4.43 ug/1 1108680 1,4 -Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanol, 1-(2-methoxy-l-methylet 148 C7H1603 020324-32-7 90 2 2-Butanol, 3,3’-oxybis- 162 C8H18O3 054305-61-2 64 3 2-Propanol, 1-(2-methoxypropoxy)- 148 C7H1603 013429-07-7 50 4 1-Propanol, 2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 45 Abundance Scan 684 (11.326 mln): 29234.D (-) m/z 59.05 .00% 100.ee

A 59

5000 45 103 73 T [ I 1'1 1 1 I 1^1 1 1 I I 11 11.00 11.20 11.40 11.60 0— | l i p-r +3414—53 4——— ■ TT ■ i 83 8990 MF1 t 130 • IT i. ।।> । ।> m/z 45.00 46.46% m/z-? 20 30 40 50 60 70 80 100 110 120 130 140 Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 31 45 73 103 T T T 11.00 11.20 11.40 11.60 A 35.58%

miz-> —' I‘ ‘■I I ‘ ‘ ‘ ‘I+ 20 30 40 50 60 70 —m 80 90 100 TT--— 130 —uunur 110 120 130 140 Abundance #12859: 2-Butanol, 3.3-oxybis- 59 r "I 11.00 11.20 11.40 11.60 5000 31 45 m/z 73.0.03 27.84% 103

UA 1

-- 1 ‘ — ----- 134 1 i ■ • 1 ■ I • ■ ‘ ■ i 1 ■ ■ ■ i ' miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #9233:2-Propanol. 1-(2-methoxypropoxy)- ' ■ i ■ ‘ ‘ 1 i ‘ ‘ 59 11.00 11.20 11.40 11.60 m/z 41. OP 23.73% 5000

miz—> 31 .. ......... 1....... — 20 30 40 45

50 60 73 104 130 . t l > r. । . j . . । । . । i । ■ I . i I . . . . । . . . . j . . . b । . 70 80 90 100 110 120 130 140 UA Tl 1 | 1 1 ■ H > 1 TIT 11.00 11.20 11.40 11.60

29234.D GCMS1126.M Fri Dec 14 16:48:42 2001 Page 4

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