GCMS analysis comments, sample AD29233, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\DEC1001\29233.D Vial: 15 Acq On : 11 Dec 2001 12:23 am Operator: 209 GALOS Sample : gc/ms scan 12/3 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.

11.33 2.99 ug/1 915180 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 72 2 2-Propanol, 1,1 ′ -oxybis- 134 C6H14O3 000110-98-5 56 3 2-Butanol, 3,3’ -oxybis- 162 C8H18O3 054305-61-2 50 4 2-Propanol, 1-(2-methoxypropoxy)- 148 C7H1603 013429-07-7 50 Abundance Scan 685 (11.331 mln): 29233.D (-) m/z 59.05 10 00% 59

5000 45 103 73 11.1 11.00 11.20 11.40 11.60 _______ 39 , 53 ,1, 67 „ 83 89 ' I * * * | । * THr | rr. I | .... । I I', । j Ti l 71 .... t . • • ....... ___________ 130 i • • ■ • i ■ • ■ • i • ■ ■41 ’ m/z 45.0,0. 46.19% miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #9238:2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 103 11.00 11.20 11.40 11.60 45 73 31 m/z 103.00. 34.85% j 130 TIP I --P miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #6087: 2-Propanol. 1,1-oxybis- 59 ■ ■ i ■ ■ 1 • i ■ TTn 11.00 11.20 11.40 11.60 31 5000 45 m/z 73.00 28.11% 103

m/z-> Abundance 20 1 i • ■ • ■ i ■ T—na—T ■ r> 30 40 50 , 60

59 70 । 72 80 । 90 । 100 #12859:2-Butanol, 3,3‘-oxybis- 89 । । । । 110 । 120 । . . • > । • 130 140 * ‘ f 1 11.00 1120 11.40 11.60 m/z 41.05. NUA22.73%

11 5000 31 45 103

— # 1111 — l‘ • ' • i ■ • ‘ 1 i ‘ ‘ ‘ ■ i • ' ■'i‘ .1___________ ’ ' i ‘ 1 ' ■ i ‘ 134 ' i ■ • ' ' i ' 1 r Tr 71 1 i ‘ m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 11.00 11.20 11.40 11.60

29233.D GCMS1126.M Fri Dec 14 16:13:02 2001 Page 4

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