Laboratory analysis report for sample AD29235 conducted on December 28, 2001, including surrogate recovery data.
NYC-WTC_000036243–000036254Folder label: “GCMS X 12/4/01 A 12/10/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC1001\29294.D Vial: 10 Acq On : 12 Dec 2001 8:30 am Operator: 209 GALOS Sample : gc/ms scan 12/4 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
11.42 0.98 ug/1 245443 1,4-Dichlorobenzene-d4 11.67
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2-Propanol, 1-(2-methoxy-l-methylet 148 C7H16O3 020324-32-7 78 2 2-Butanol, 3,3' -oxybis- 162 C8H18O3 054305-61-2 50 3 2-Propanol, 1-(2-methoxypropoxy)- 148 C7H1603 013429-07-7 47 4 1-Propanol, 2 -(2-hydroxypropoxy) - 134 C6H14O3 000106-62-7 45 Abundance / Scan 695 (11.424 min): 29294.D (-) m/z 59.05 100.00% 59
m/z--> 5000 -
20 30 40 45
—lL—r50----- 60 —4+ 70I 80 73
85..... j................ 90 100 110 120 130 140 m/ z 103
11.00 11.20 N 11.40 44.9,5 11.60 11.80 50.69% Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59
5000- । , . ( ' * | - • ■ ■ | > . k ■ | • 45 103 11.00 11.20 11.40 11.60 11.80 73 31 m/z 103.05 39.21% ----------- • l ■ ■ • 1 | ■ ■ ■ • । > ■ ■ ■ । ■ ■ ■ > । 130 ■ t > i miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol. 3,3‘-oxybis- 59 0 ........ TIITT 11.00 11.20 11.40 11.60 11.80 5000- 31 m/ z 73.00 27.20% I 45 103 i
, 134 1I1 ■ i • ■ ■ ■ i ■ ‘ ■ i • ■ • ■ I ■ 1 1 ■ I ■ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #9233: 2-Propanol, 1-(2-methoxypropoxy)- T —r T‘‘Ek । । । । । । । । । 59 11.00 11.20 11.40 11.60 11.80 m/ z 5000
31 45 73 ---------- T1t1111*1 104 ——‘IETTTTTurriu ‘11111OI 130 —*R 1 I ■ • ' 1 TTI । । । । । m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 11.00 11.20 11.40 11.60 11.80
29294.D GCMS1126.M Wed Dec 19 12:55:56 2001 Page 4
NYC-WTC_000036253
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NYC-WTC_000035853
Lab notes for sample AD29139 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036114
Laboratory report noting GCMS scan results for sample AD29230 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036103
Laboratory report noting GCMS scan results for sample AD29189 with di-n-butylphthalate detected and low pH.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036220
Blank sample results showing non-detect levels for target compounds during December 2001 laboratory testing.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036278
Laboratory analysis report for sample AD29296 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036325
Laboratory GCMS analysis report for sample AD29229 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035919
Laboratory report noting detection of di-n-butylphthalate in sample AD29025 analyzed on December 18, 2001.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035831
Lab notes for sample AD29141 indicate detection of bis(2-Ethylhexyl)phthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036289
Laboratory analysis report for sample AD29455 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035978
Laboratory report noting detection of di-n-butylphthalate in sample AD29026 analyzed on December 18, 2001.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035865
Lab notes for sample AD29134 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035808
Laboratory analysis notes for sample AD29023 indicating no unusual compounds detected in GCMS scan; one of forty-three compounds in quality control standard outside acceptance rang
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000036199
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000036200
Laboratory methodology table documenting sample extraction parameters, surrogate recovery rates, and quality control data for mass spectrometry analysis.
Filed in the same folder
NYC-WTC_000036201
Laboratory record documenting the extraction method parameters for sample AD29229 analyzed in December 2001.
Filed in the same folder
NYC-WTC_000036205
Calibration data for volatile organic compounds including nitrosamines and chlorinated solvents from December 2001.
Filed in the same folder
NYC-WTC_000036210
Reference analysis results for target analytes used to verify GCMS instrument performance in December 2001.
Filed in the same folder