GCMS analysis results sample AD29460, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD29460 conducted on January 4, 2002, showing unknown compounds and surrogates.

NYC-WTC_000036458–000036468

Folder label: “GCMS X 12/5/01 A 12/12/01”

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NYC 9/11 Public Portal Document

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Data File : C:\HPCHEM\l\DATA\DEC1201\29460.D Vial: 19 Acq On : 12 Dec 2001 8:33 pm Operator: 209 GALOS Sample : gc/ms scan 12/5 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.42 1.45 ug/1 408597 1,4-Dichlorobenzene-d4 11.68

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-2-methoxy-1-methylet 148 C7H1603 020324-32-7 83 2 2-Butanol, 3 ,3 ' -oxybis- 162 C8H18O3 054305-61-2 64 3 1-Propanol,/2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 59 4 2-Propanol/ 1-(2-methoxypropoxy)- 148 C7H1603 013429-07-7 40

AA Abundance Scan 694 (11.418 min): 29460.D (-) m/ z 59.05 100.00% 59

5000 45 103 73 11.00 11.20 11.40 11.60 11.80

m/z—> c 20 -51 30 40 50 60 70 --- 80 90 100 । ■ • ■ ■ । ■ • ■ ■ । • ■ ■ • । ■ 110 120 130 140 m/ z 45.0.0 47.71% Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxyl 59

5000- 45 103 11.00 11.20 11.40 11.60 11.80 73 31 m/z 103.05 35.94% ..... i........... 130..... ■ i ' 1 1 ■ i ' 1 ■ ' i 1 ■ i ■ ■ • ■ I ■ ■ • ■ । । m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859; 2-Butanol, 3,3°-oxybis- 59 — ————— , IdTT 11.00 11.20 11.40 11.60 11.80 5000- 31 m/z 73 00 26.42%

A 45 103 I

.1 134 1 I ' ' ' ■ 1 1 ' ' ' 1 1 ■ i ■ ■ ■ > i • ■ ■ • i ■ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 V Abundance #6086: 1-Propanol, 2-(2-hydroxypropoxy)- T —y ■ ■ i • ■ > ■ i > ■ • ■ । > 59 11.00 11.20 11.40 11.60 11.80 m/z 41.05 24.60% 5000 31 45 103 - 89 —T ' i ' 75. ' ' ' i ' ' ' ' i 1 ' ■ ' i ' 1 ■ ' i ' ' ' ' I ' ' ' ' i ' ' ' ■ i ‘ T-f-r-r-n-) ‘rnk—n.r m/z-> 20 30 40 50 (60 70 80 90 100 110 120 130 140 11.00 11.20 11.40 11.60 11.80

29460.D GCMS1126.M Fri Dec 21 12:27:42 2001 Page 3

NYC-WTC_000036467

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NYC-WTC_000036467Source: NYC Law Department, mirrored locally

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GCMS analysis results sample AD29297, Jan 2002 · Box DEP Box 22

NYC-WTC_000036380

Laboratory report documenting GCMS analysis of sample AD29297 conducted on January 4, 2002, showing unknown compounds and surrogates.

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