GCMS analysis results sample AD29462, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD29462 conducted on January 4, 2002, showing unknown compounds and surrogates.

NYC-WTC_000036480–000036490

Folder label: “GCMS X 12/5/01 A 12/12/01”

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NYC 9/11 Public Portal Document

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Data File : C:\HPCHEM\l\DATA\DEC1201\29462.D Vial: 22 Acq On : 12 Dec 2001 11:28 pm Operator: 209 GALOS Sample : gc/ms scan 12/5 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.43 0.66 ug/1 158649 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

12-Propanol, 1-(2-methoxy-l-methylet 148 C7H16O3 020324-32-7 72 22-Butanol, 3,3' -oxyis- 162 C8H18O3 054305-61-2 64 32-Propanol, 1,1' -oxybis- 134 C6H14O3 000110-98-5 56 42-Propanol, 1- (2/methoxypropoxy) - 148 C7H16O3 013429-07-7 47 Abundance 7 Scan 696 (11.431 min): 29462.D (-) m/z 59.05 1 0.00% 59

, m/z-> 5000-

' i ■ ■ ■ 1 i 1 ' 1 20 30 40 45

!50 1——— 60 TH 70 73

i'■ ■ i ■ ■ • • i ■ • • ■ T 80 90 100 103

। 110 । 120 । 130 । . 140 m/z N 11.20 11.40 11.60 11.80 44.95 ■ ■ i ■ •

44.77% 'Abundance #9238: 2-Propanol, 1 -(2-methoxy-1 -methylethoxy} 59

5000 - 45 103 11.20 11.40 11.60 11.80 73 31 m/z 102.95 33.38% ........... ।.......... 130 — • i > ■ ■ ■ I • ■ ■ ■ i ‘ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 ■Abundance #12850: 2-Butanol. 3,3°-oxybis- 59 T ——P 11.20 11.40 11.60 11.80 5000 - 31 45 m/z 73.00 27.61% 103

TT’Irrdr । i , । rI _______ .._______________________________________ T-r-f-r-rT-r-p-TT-j-j- , . T 134 i i f i i i i । i i i i j i m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 ’Abundance #6087: 2-Propanol, 1,1’-oxybis- T—IUr TT I I ... I I I I I 59 11.20 11.40 11.60 11.80 m/ z 41.00 22.95%

_NA 31 5000 45 103 — — । ... I 89 H 1 i721 1 1 ■ r1 1 r 1 | i 1 1 1 1 i TIr +-PA44 -............. m/z-> 20 30 40 50 (60 70 80 90 100 110 120 130 140 11.20 11.40 11.60 11.80

29462.D GCMS1126.M Fri Dec 21 12:29:54 2001 Page 3

NYC-WTC_000036489

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GCMS analysis results sample AD29461, Jan 2002 · Box DEP Box 22

NYC-WTC_000036469

Laboratory report documenting GCMS analysis of sample AD29461 conducted on January 4, 2002, showing unknown compounds and surrogates.

1 shared topics · Same agency, volume and box · similarity 0.999