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GCMS analysis comments for sample AD29141, Dec 17 2001

Machine-extracted title · confidence 95%

Lab notes for sample AD29141 indicate detection of bis(2-Ethylhexyl)phthalate and one LCS compound outside acceptance range.

NYC-WTC_000035831–000035842

Folder label: “GCMS X 11/30/01 A 12/10/01

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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1001\29141.D Vial: 8 Acq On : 10 Dec 2001 5:34 pm Operator: 209 GALOS Sample : gc/ms scan 11/30 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

11.35 0.46 ug/1 111731 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxy-l-methylet 148 C7H1603 020324-32-7 72 2 2-Butanol, ,3 1 -oxybis- 162 C8H18O3 054305-61-2 50 3 2-Propanol, 1,1’-oxybis- 134 C6H14O3 000110-98-5 50 4 1 - Propanol , 2 - (2 - hydroxypropoxy) - 134 C6H14O3 000106-62-7 45 Abundance Scan 686 (11.346 min): 29141 .D (-) m/ z 59.05 100,.00%

5000 45 59

73

85 103

। . TrtT . । i ri i । i i i i TTTT i । i i i i । i i i i-j i i i i । i ■ ■ i 1 ■ A ‘ T ‘ ‘ 1 ’ I 1 ‘ 11.00 11.20 11.40 11.60 m/z 44.95 ‘ I ' * ‘ ‘ 1 ‘

49.51%

N miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance J #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 45 103 T Tr ————— 1 ‘ 1 1 ‘ ’ • t * * ' ‘ I ‘ 73 11.00 11.20 11.40 11.60 31 m/z 103.05 33.38% 130 m/z~> 20 ‘30 “ 40 —H। I' 1' 1 11 — PPP ■ ■ i ■ 1 ■ ■ I 1 1 1 1 1 1 50 (60 70 80 90 100 110 120 130 140 Abundance #12859; 2-Butanol. 3,3’-oxybis- 59 T T ri 11.00 11.20 11.40 11.60 5000 31 m/z 73.00 27.93%

N 45 103

-----......... —........................ 134,, . miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #6 37: 2-Propanol, 1,1-oxybis- ‘ « I •• TT 1—.—//— J i 519 11.00 11.20 11.40 11.60 m/z 41.00 22.57% 31 5000

tnlz~> 20 30 40 45

72 — TIT61-7112199*2615186111TTOI5*TITTI1T 50 60 70 80 90 100 110 120 130 140 103 NN d1d 28.T 118T TIn TGIFTTTT J 1 11.00 11.20 11.40 11.60

29141.D GCMS1126.M Wed Dec 12 16:08:33 2001 Page 3

NYC-WTC_000035840

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NYC-WTC_000035840Source: NYC Law Department, mirrored locally

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