GCMS analysis results for sample AD30354, Jan 2002

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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30354 conducted on January 10, 2002.

NYC-WTC_000017796–000017807

Folder label: “GCMS X 12/13/01 A 12/27/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C: \HPCHEM\ 1 \DATA\DEC2 701\30354.D Vial: 6 Acq On : 27 Dec 2001 4:03 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

11.35 0.42 ug/1 153703 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 72 2 2-Butanol, 3,3' -oxybis- 162 C8H18O3 054305-61-2 64 3 2-Propanol, 1,1' -oxybis- 134 C6H14O3 000110-98-5 50 4 1-Propanol, 2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 42 Abundance Scan 687 (11.354 min): 30354.D (-) m/z 59.05 100.00% 59

I 5000-

’11’1111 „ll 45

85 91 , 103

’l| ri11 1TTuest1—n1—1—03111111111I11-’1T NJ TnnmrmuutIuu—IOwu—r 11.00 11.20 11.40 11.60 m/ z 45.05, 56.27%

5 f*T-rr miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #9238:2-Propanol, 1-(2-methoxy-1-methylethoxy) 59

5000 103 • l ‘ • 45 11.00 11.20 11.40 11.60 73 31 m/z 103.05 33.60% ‘ | ‘ l i 130 ' i ■ ‘ ■ i ■ ■ • • t1 miz-> 20 30 40 50 (60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol. 3.3’oxybis- 59 ‘ i ■ ‘ «i.111* 11» । . k j i 11.00 11.20 11.40 11.60

A 5000 31 45 m/z 73.00 26.57% 103

( i , ■।• • "i ■■• ■ । 11 ' ■I' ■ ‘ ■ i •1• ' i 1 • ‘ 1i ■ ■ ‘ • i * ■■• i ‘ 134 ■i1 1 • ‘ i ■•■ * i 1 ■ ■'i ' miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #6087:2-Propanol, 1,1’-oxybis- : 59 11.00 11.20 11.40 11.60 m/ z 41.00. 23.66%

3 31 5000 45 103 89

m!z-> • i ■ ■ ■' । 20 30 ■11' 40 50 1’(60 m2 “I 70 romaapansar TTuTTT 80 90 100 110 120 130 140 -KdnmmmnCB——rr 11.00 11.20 11.40 11.60

30354.D GCMS1126.M Wed Jan 02 10:54:00 2002 Page 3

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