GCMS analysis comments, sample AD29137, Dec 2001

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1001\29137.D Vial: 33 Acq On : 11 Dec 2001 7:54 pm Operator: 209 GALOS Sample : gc/ms scan ll/30a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Propanol, 1-(2-methoxy-1-met Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

11.43 0.64 ug/1 178802 1,4-Dichlorobenzene-d4 11.67

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanol, 1-(2methoxy-1-methylet 148 C7H1603 020324-32-7 72 2 2-Butanol, 3,3%-oxybis- 162 C8H18O3 054305-61-2 64 3 2-Propanol, 1,1′-oxybis- 134 C6H14O3 000110-98-5 50 4 2-Propanol,Zl-(2-methoxypropoxy)- 148 C7H16O3 013429-07-7 40

MX Abundance Scan 696 (11.433 mln): 29137.D (-) m/ z 59.05 100.00% 59 45 5000 103 73 "11 ■ r I l I I I I I 1 1 I I I > 1 > 11.20 11.40 11.60 11.80

miz-> ... 20 30 .40 50 l— .70T+T 60 .. ..85 > । i r. . । 80 . । T।। . TT — m/z 45.05 ‘ i • ‘ 90 100 110 120 130 140 53.38% • i ■ ‘ 1 1 I ■

Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy) 59

5000 103 45 73 31 m/z 103.00 36.44% ....... 130.... 'sb' ’' H i60 701— -IP P T ।. 11.. miz-> 20 30 40 80 90 100 110 ' 120 130 140 Abundance #12859: 2-Butanol. 3,3-oxybis- 59 •11 h 1 ■ ’111 ■ ■ ■ i1 • TTr 11

AC 11.20 11.40 11.60 11.80 5000 31 45 m/z 73.00 30.63% 103

■ । ■ • • • । ■ ■ ■ ■ । ‘ .... ..................... ....... .. miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #6087: 2-Propanol, 1,1‘-oxybis- 59 11.20 11.40 11.60 11.80 m/z 41.05 25.10% 31 45

JA 5000 103

72 89 I T I » I I T 11III TTIT TT I 1 I 1 1 1 ‘ | । i > i'i । i > > । ■1 ■ ■ । • ■ ■ • । ‘ । ■ ■ ■ • । •

m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 11.20 11.40 11.60 11.80

29137.D GCMS1126.M Wed Dec 12 15:54:40 2001 Page 4

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