GCMS analysis comments, sample AD29234, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1001\29189.D Vial: 20 Acq On : 11 Dec 2001 5:15 am Operator: 209 GALOS Sample : gc/ms scan 12/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

11.34 0.79 ug/1 172936 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 83 2 2 -Butanol, 3,3’ -oxybis- 162 C8H18O3 054305-61-2 64 3 1-Propanol, 2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 42 4 2-Propanol, 1,1'-oxybis- 134 C6H14O3 000110-98-5 40 Abundance Scan 686 (11.339 mln): 29189.D (-) m/z 59.05 10C .00% 59

miz-? 5000

20 ■ i ■ ■ • • I 1 1 30 .911 40 45

—5051—460— TI70’f • 80 73

T'■ 103

90 100 110 120 130 140 i1 ■ ■ • i • • •11 • ■ ■' i ■ T Ju 11.00 11.20 11.40 11.60 m/z 44.95 47.86% T

Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy> 59

5000 103 1 1 I ‘ T T T T 45 11.00 11.20 11.40 11.60 73 31 m/z 102.95 34.83% — I TI — PITT । — । T »i - .................. 130......... miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol, 3,3°-oxybis- 59 T ■i 1 r i T T 11.00 11.20 11.40 11.60 5000 31 m/z 73.00 29.07% -.v,s

NA 45 103

134 — i | i | | 'rf i • । ( i । । . i । । । । . miz—> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #6086: 1-Propanol, 2-(2-hydroxypropoxy)- * * I * » * * 1 » T—BO— 59 11.00 11.20 11.40 11.60 m/z 41.05, 25.65%

m/z—> 5000 31 45

—I — — ' ‘' I + 11 r T’l tur • i * 75 20 30 40 50 60 70 89 103

■' ■ i ■ ■ • ■ i ■ • ■ ■ । •1 ■ • ।■ i1 ■ ■ ■ i ■ • ■ ■ i ■ 80 90 100 110 120 130 140 NA —Pfrfrr TII Fnn t I l i I 11.00 11.20 11.40 11.60

29189.D GCMS1126.M Fri Dec 14 16:07:40 2001 Page 2

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