GCMS analysis comments, sample AD29287, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1001\29287.D Vial: 17 Acq On : 11 Dec 2001 2:20 am Operator: 209 GALOS Sample : gc/ms scan 12/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.42 1.07 ug/1 282004 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 90 2 2-Butanol, 3,3’-oxybis- 162 C8H1803 054305-61-2 50 3 1-Propanol, 2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 45 4 2-Propanol, 1,1'~[(1-methyl-1,2-eth 192 C9H20O4 001638-16-0 42 Abundance’ Scan 694 (11.419 min): 29287.D (-) m/z 59.05 100.00% 59

5000

39 11PITI 45

44—51 —— 4 73 89 103

-PP 130 ..M 11.00 11.20 11.40 11.60 11.80 45,00 1 ■ I ‘ '

NX • i 1 • । 'i ■ TT 130' ’ 140 m/z 44.81% miz-? 20 30 40 50 60 70 80 90 100 110 . 120 Abundance #9238:2-Propanol, 1-(2-methoxy-1-methylethoxy} 59

5000 103 T T T T f 45 73 11.00 11.20 11.40 11.60 11.80

.V 31 ----- TIH ' 1 1 IT *II___________ 130 T[in I I I J TT ! I 1UI TT[B miz-> 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butarol. 3.3°oxybis- 59 । । । i rpi 1 > I I > I I I I I 1111— 11.00 11.20 11.40 11.60 11.80 5000 31 45 m/z 0.0 73.00 28.14% -.-t

NA 103

4 r : P i — * i ■ ' ‘ ‘ I,•............... ,............ 134 ■ ‘ • i • ■ ■ 1 i • ■ • ■ i ‘ ■ • • i ■ • ■ • i ■ ■ ■ ■ i ■ ■ ‘ • i1 । ■ 11 1 miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #6086:1-Propanol, 2-(2-hydroxypropoxy)-

5000

miz—> 20 31

30 40 45

ii 59

75 * I '* * • I * ‘: j li. . । . TH — ——— TuIputt—tpn i ■ , IT 50 60 70 80 89 90 103

100 110 120 130 140 m/z

"1RPUIT NA 11.00 11.20 11.40 11.60 11.80 41.05

11.00 11.20 11.40 11.60 11.80 25.13%

29287.D GCMS1126.M Fri Dec 14 16:14:24 2001 Page 3

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