GCMS re-analysis comments, sample AD29232, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1001\29232.D Vial: 16 Acq On : 11 Dec 2001 1:22 am Operator: 209 GALOS Sample : gc/ms scan 12/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

11.41 2.72 ug/1 750774 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual l 2-Propanol, 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 78 2 2-Propanol, 1-(2-methoxypropoxy)- 148 C7H1603 013429-07-7 50 3 2-Butanol, 3,3'-oxybis- 162 C8H18O3 054305-61-2 50 4 1-Propanol, 2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 45 Abundance Scan 694 (11.412 mln): 29232.D (-) m/z 59.05 100.00%

5000

21-51 45

——— 85 91 1 73

130 TT* HIT TTIPTTTT , TIOOYDT—upr m/z 103 _M 11.00 11.20 11.40 11.60 11.80 45.00 47.25% TTT

miz-? 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #9238:2-Propanol, 1-(2-methoxy-1 -methylethoxy }

5000 31 45 59

73 103 A V I ■ ' ■ ‘ I ' 1 1 ' I ' ’ I ‘ I 1 ' ' 1 r1 1 11.00 11.20 11.40 11.60 11.80 m/z 103.0. 36.31% — pt --- 130 (i •(1 ■ TTT ' * i1 miz-> 20 30 40 50 (60 70 80 90 100 110 ' 120 130 140 Abundance......... #9233; 2-Propanol 1 -(2-methoxypropoxy)- 59 i ■ ■1 m ■ TTT TTIr 1 11.00 11.20 11.40 11.60 11.80 5000 m/z 73.00 2 7.93%

m/z-> Abundance 20 31 ................... L 30 45 3 I’ 1628.8 CCdod.n I I 5 40 50 —m 60 #12859:2-Butanol, 3,3‘oxybis- 59 70 73

80 130 Tgnn. I J II' r I LOSrTgt t I I I T T TT T 90 100 104 110 120 130 140

m/z M 11.00 11.20 11.40 11.60 11.80 41.0 23.59% 5000 31 45 103

134 -- 1′011 TTTT , t > ! . . | TTmnprr TITT ' '"I 1 m i # ■ ■ I 14 1mmT 1 • ‘ i 1 1 ‘ ■ i ' ‘ ‘ • i ■ • • ■ i ‘ m/z—> 20 30 40 50 I60 70 80 90 100 110 120 130 140 11.00 11.20 11.40 11.60 11.80

29232.D GCMS1126.M Fri Dec 14 16:11:20 2001 Page 3

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