GCMS analysis comments, sample AD29230, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC1001\29230.D Vial: 18 Acq On : 11 Dec 2001 3:18 am Operator: 209 GALOS Sample : gc/ms scan 12/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-1-met Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

11.33 2.31 ug/1 669867 1,4-Dichlorobenzene-d4 11.67

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanol, 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 72 2 2-Butanol, 3,3’ -oxybis- 162 C8H18O3 054305-61-2 64 3 2-Propanol, 1-(2-methoxypropoxy)- 148 C7H16O3 013429-07-7 50 4 1-Propanol, 2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 42 Scan 685 (11.334 min): 29230.D (-) m/z 59.05 100.00% 59

5000 45

39.1 51 , । । i >i । । । । i 14 . i . * +4— ■ ‘ TH 73

--99---- 103

130 1 ' I 1 ■ • ■ i ' ■ MX 11.00 11.20 11.40 11.60 m/z 45.05 46.32% miz-2 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 45 73 103 11.00 11.20 11.40 11.60 ' ‘ r 31 m/z 103.00 34.41% . । m . TI TH I* — 130 TIt — —Ir • • । i • miz-> 20 30 40 50 60 70 80 90 100 118 120 130 140 Abundance #12859: 2-Butanol, 3 3’-oxybis- 59 i . ! > i { I ... । . ... | . , "T 11.00 11.20 11.40 11.60 5000 31 m/ z 73.00. 27.74%

"A 45 103

-----..... -134 miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #9233: 2-Propanol, 1-(2-methoxypropoxy)- TT-pr-T 59 11.00 11.20 11.40 11.60 m/ z 41.055 21.05% 5000

m/z-> 31 I. 45 in | _ 3 T-p-rT-> । . . . . 1′11′18 1 1 * I'' • • । । 20 30 40 50 60 70 । 80 104 130 ‘ ■ i ■ ■ ' • i ■ * ‘ ‘ i • ■ ■ • i ■ • ' ‘ i ■ ‘ 90 100 110 120 130 ' i * 140 ..Il 11.00 11.20 11.40 11.60

29230.D GCMS1126.M Fri Dec 14 16:09:01 2001 Page 3

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