GCMS analysis comments, sample AD29230, Dec 2001

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1001\29230.D Vial: 18 Acq On : 11 Dec 2001 3:18 am Operator: 209 GALOS Sample : gc/ms scan 12/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.42 3.01 ug/1 872957 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanol, 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 90 2 2-Butanol, 3,3'-oxybis- 162 C8H1803 054305-61-2 56 3 1-Propanol, 2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 42 4 2-Propanol, 1-(2-methoxypropoxy)- 148 C7H16O3 013429-07-7 25 Abundance Scan 694 (11.417 mln): 29230.D (-) m/z 59.05 100.00% 59

5000

39 45 73 103 ... M. 11.00 11.20 11.40 11.60 11.80 1444—53.—— 130 70 +399—— i • ■ ■ ■ i • • ■ ■ I 1 ■ • ■ i ■ m/ Z 44,95 45.26%

UA m/z-> 20 30 40 50 60 80 90 100 110 120 130 140 Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy,- 59

5000 r- 1 r TI 1 1 45 103 11.00 11.20 11.40 11.60 11.80 73 31 m/z 103.05 36.46% — - ----PP .......... 130........ miz—> 20 30 40 50 60 70 80 90 100 110 120 130 14 Abundance #12859: 2-Butanol. 3 3‘-oxybis- 59

11.00 11.20 1140 11.60 11.80 5000 31 45 m/ z 73.00 28.92%

NA 103

m/z-> 20__ 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #6086: 1-Propanol, 2-(2-hydroxypropoxy)- T1.7 59 11,00 11.20 11.40 11.60 11.80 m/z 41.05 23.31% 5000

m/z-> 31 45 75 89 103

...................... II,I, , , , T or TIETt*111111I11*00IS 20 30 40 50 60 70 80 90 ——IVICI6TT1gs 100 110 120 130 140 £l I* 1 1 1 I iii । । i i‘‘| » T r<pT' 11.00 11.20 11.40 11.60 11.80

29230.D GCMS1126.M Fri Dec 14 16:09:05 2001 Page 4

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