GCMS analysis comments, sample AD29140, Dec 2001

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1001\29140.D Vial: 37 Acq On : 11 Dec 2001 11:46 pm Operator: 209 GALOS Sample : gc/ms scan 11/30a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.43 0.53 ug/1 146592 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanol, 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 83 2 2-Propanol, 1,1’ -oxybis- 134 C6H14O3 000110-98-5 56 3 2 - Propanol, 1 - (2-m e thoxypropoxy) - 148 C7H1603 013429-07-7 47 4 2-Butanol, 3,3'/oxybis-___ 162 C8H18O3 054305-61-2 39

NN. Abundance Scan 696 (11.431 mln): 29140.D (-) m/z 59.05 100.00% 59

5000 45 73 103 11.20 11.40 11.60 11.80 -31 4. l

.N .. . 86 TTTT m/ z 44.95 46.28% mz-A 30 40I 50 60 70 80 90 100 110 120 130 Abundance #9238:2-Propanol, 1-(2-methoxy-1-methylethoxy>• 59

5000 103 45 73 11.20 11.40 11.60 11.80 31 m/z 102.95 34.05% 1 ■ • i • ■ ■ • । • । TP+ —t 111 1 1 ' 1 1 1 P 130 ■ ' i • miz-> 30 40 60 70 50 1 80 90 100 110 120 130 (Abundance #5087- 2-Propanol. 1,1-oxybis- 59 i -NR* ■ ■ i ■

31 11.20 11.40 11.60 11.80

M 5000 45 m/z 73.00 27.92% 103 72 89 ; 1101111 l-T-p-r i ‘ ' 1 i ‘ ' i ‘ ■ i • ‘ ‘ ■ i ' ‘ ‘ ‘ I TTgTTTIT m/z-> 30 40 50 60 70 80 90 100 110 120 130 Abundance " #9233: 2-Propanol, 1-(2-methoxypropoxy)- Tmam*uuuii)i 59 11.20 11.40 11.60 11.80 m/z 41.05 23.25%

miz-> 5000-

31 45 73 | '11 r11 > i j> ’ 4 ------ • • i • 30 40 50 60 70 80 90 104 100 110 120 130 130 _N 11.20 11.40 11.60 11.80

29140.D GCMS1126.M Fri Dec 21 15:07:52 2001 Page 3

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