GCMS analysis comments for sample AD29022, Dec 17 2001

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Library Search Compound Report

Data File : C: \HPCHEM\ 1 \DATA\DEC10 01\29022.D Vial: 9 Acq On : 10 Dec 2001 6:33 pm Operator: 209 GALOS Sample : gc/ms scan 11/30 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanol, 1- (2-methoxy-1-met Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

11.35 0.45 ug/1 110076 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 83 2 2-Propanol, ,1 ' -oxybis- 134 C6H14O3 000110-98-5 50 3 1-Propanol,/2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 45 4 2-Propanol, 1-(2-ethoxypropoxy) - 162 C8H18O3 010143-32-5 39 Abundance Scan 687 (11.354 mln): 29022.D (-) m/z 59.05 10 .00% 59

5000 45 73 103 . TPTIT

miz-? —l +51- 30 40 50 60 70 89 1* « ‘T1 80 90 ■ i • 100 • i ■ ■ ■ ■ i 1 ■ • 1 i ‘ 110 120 130 11.00 11.20 11.40 11.60 m/z 45.05 45.40% Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 103 45 73 11.00 11.20 11.40 11.60 31 m/z 103.05 34.97% 1 1 — ---—PTT FIPTT 130 m/z-> 30 40 50 160 70 80 90 100 110 120 130 Abundance #6087; 2-Propanol. 1,1-oxybis- 59 II—fr । i /1 । > > i i । i TP 11.00 11.20 11.40 11.60 31 5000 45 m/z 73.00 29.49% 103 72 89 • i • • • • i • TTT । . . « . । • TITTTITTITI m/z-> 30 40 50 60 70 80 90 100 110 120 130 Abundance #6086:1-Prropaand. T-J-T ’itt IT r-f-r-T-r-n . ( . . . . । . 59 11.00 11.20 11.40 11.60 m/z 41.05 24.21%

jU 5000 31 45 103

— P 4— —+—tr ' I ' 75 ' ‘ ‘ I ‘ 89 ‘ I • ' ' ‘ I ‘ 1 ' ‘ I ' ‘ ‘ I 1 ‘ ‘ ‘ I ‘ 1 “1—Y miz—> 30 40 50 160 70 80 90 100 110 120 130 11.00 11.20 11.40 11.60

29022.D GCMS1126.M Wed Dec 12 16:03:23 2001 Page 2

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