GCMS sample analysis results, Jan 2002

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Data File : C:\HPCHEM\1\DATA\DEC2101\30313.D Vial: 14 Acq On : 22 Dec 2001 7:31 pm Operator: 209 GALOS Sample : gc/ms scan 12/13a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.44 0.50 ug/1 141439 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, (2-methoxy-1-methylet 148 C7H16O3 020324-32-7 72 2 2-Propanol, 1,11 -oxybis- 134 C6H14O3 000110-98-5 56 3 1-Propanol/ 2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 53 4 2-Butanol/ 3,3’-oxybis- 162 C8H18O3 054305-61-2 50 Abundance Scan 696 (11.437 min): 30313.D (-) m/z 59.05 100.00% 59

5000

39 .1 -P+ 1511/.... "1 45

73

85 r' ■ i ■ ■ ■ ■ i ■ 103

IMea m/z JU 11.20 11.40 11.60 11.80 44.95 ■ ■ i ■ ■

55.66% m/z-> 30 40 50 60 70 80 90 100 110 120 130 'Abundance #9238: 2-Propanol, 1-2-methoxy-1-methylethoxy)

5000 103 45 73 11.20 11.40 11.60 11.80 31 m/z 103.05 33.27% --P— 80 "90“ 100'110 130 m/z—> 30 40 50 I60 70 120 ’ 130 Abundance #6087 2-Propanol, 1,1-oxybis- 59

11.20 11.40 11.60 11.80 31 5000 45 m/ z 73.00 26.23%

miz-> Abundance ■ 1 72 89 I1I1111****11* 30 40 I

50 60 59 70 80 90 103

100 #6086:1-Propanol, 2-(2-hydroxypropoxy)- 110 120 130 TTfr

m/z MJ 11.20 11.40 11.60 11.80 41.00 23.04% .043

m/z-> 5000 31

_________ 11 ■ ■ i ■ • ■ ■ 1 1 30 40 45

50 PTT T1BB75 I60 70 89 —mmmammmu 80 ——u——uur 90 103

100 110 120 130 NA • ■ i 1 ■ ■ 1 I 1 1 1 ' I 1 1 1 1 I ' 1 11.20 11.40 11.60 11.80

30313.D GCMS1126.M Wed Jan 02 10:17:16 2002 Page 3

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