GCMS analysis results for sample AD31461, Feb 11, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN1602\31461 .D Vial: 29 Acq On : 17 Jan 2002 4:00 pm Operator: 209 GALOS Sample : gc/ms scan 12/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.27 0.52 ug/1 121123 1,4-Dichlorobenzene-d4 11.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 72 2 2-Propanol , 1,1' -oxybis- 134 C6H14O3 000110-98-5 56 3 1-Propano1, 2-(2-hydroxypropoxy)- 134 C6H1403 000106-62-7 53 4 2-Butanol, 3,3'-oxybis- 162 C8H18O3 _ 054305-61-2 36 Abundance Scan 678 (11.272 mln): 31461 .D (-) m/z 59.05 100.00% i

5000

39 1 45 59

. 84 73

I, 103

1gri" 11 '-■■i ■ ’ll—t 1 ■ • i ■ 1 ■ ■ i ■ ' ■ ' i ■ 1 • • i ■ ■ ■ 1 I ■ ■ ■ ■ i ■ • _.M11.00 11.20 11.40 11.60 m/ z 45.00 49.45%

MA miz-> 30 40 50 I60 70 80 90 100 110 120 130 Abundance #9238:2-Propanol, 1-(2-methoxy-1-methylethoxy}- 59

5000 45 73 103 11.00 11.20 11.40 11.60 31 m/z 103.00 29.84% t TIrI. | ■ ■ ■ ■ l i'« -IITT 130 m/z-> 30 40 50 60 70 80 90 100 110 120 130 Abundance >■ p 1, ilcxybis- 59

31 11.00 11.20 11.40 11.60

.M 5000 45 m/z 73.00 29.17% 103 72 89 ■ 1 1 ■ i ■ • • ■ i 1 ■ ■ ■ i ' ■ m/z~> 30 40 50 60 70 80 90 100 110 120 130 Abundance #6086: 1-Propanol, 2-(2-hydroxypropoxy)- i 59 11.00 11.20 11.40 11.60 m/ z 41.05 28.85% 5000

miz—> 31

30 40 45

50 Tr I60 75 ' i ■ ■ ‘ ■ i ' 70 80 89 103

■ i ■ ■ ' ' i ' 1 ' ■ i ' 1 1 ' i ■ ■ ■ ■ i ■ ' 90 100 110 120 130 k ' ‘ ■ 1 1 ' • ■ I ‘ 11.00 11.20 11.40 11.60 ' I ‘ '

31461.D GCMS0103.M Thu Feb 07 12:38:47 2002 Page 3

NYC-WTC_000016339