GCMS analysis results for sample AD30353, Jan 2002

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30353.D vial: 17 Acq On : 28 Dec 2001 3:42 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

11.35 0.59 ug/1 216086 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 78 2 1-Propanol, 2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 59 3 2-Propanol , 1,1’ -oxybis- 134 C6H14O3 000110-98-5 56 4 2-Butanol, 3,3'-oxybis- 162 C8H18O3 054305-61-2 50 Abundance Scan 687 (11.349 mln): 30353.D (-) m/z 59.05 100..00% vvo 59

5000

...... w. Y... 4.. 45 73

TT 1 Imp 84 103 • • 1 * M) r1 1 ' ■ i 1 1 1 1 i 1 1 1 1 । ' 11,00 11,20 11.40 11,60 m/z 45.00. 54.41% miz-> 30 40 50 60 70 80 90 100 110 120 130 Abundance #9238:2-Propanol, 1-(2-methoxy-1 -methylethoxy)

5000 " ■ r1"1 TI ' 1 i 1 1 i > i । • । . । > 45 103 11.00 11.20 11.40 11.60 73 31 m/z 103.05. 32.97% 130 • ‘ ′′* . . । I .L . । ... I TTT sigueneeka ' i ' ‘ ■ i ' ' ‘ 1 i • ■ miz--> 30 40 50 I60 70 80 90 100 110 120 130 Abundance #6086; 1-Propanol, 2-{2-hydroxypropoxy)- 59 11.00 11.20 11.40 11.60 ‘1 ‘

.N 5000 m/z 73.00 28.19% 31 45 103

75 89 /114‘* 'T‘ 1′414 ITTI I r I . I I | I . . m/z-> 30 40 50 60 70 80 90 100 110 120 130 Abundance #6087:2-Propanol, 1,7oxybis- 11.00 11.20 11.40 11.60

. NA m/z 41.00 27.49% 31 5000 45 103 72 89 ■ ■ i ■ ■ ■ ■ i1 181 1 >-T-l4H— ■ i 1 ‘ 1 1 i ‘ 1 1 1 1 i 1 ■ 1 1 i 1 = m/z-> 30 40 50 160 70 80 90 100 110 120 130 11.00 11.20 11.40 11.60

30353.D GCMS1126.M Wed Jan 02 10:52:40 2002 Page 2

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