GCMS analysis results for sample AD30353, Jan 2002

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Data File : C:\HPCHEM\1\DATA\DEC2701\30353.D Vial: 17 Acq On : 28 Dec 2001 3:42 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.43 0.90 ug/1 330638 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanol, 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 72 2 1-Propanol, 2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 59 3 2-Propanol, 1,1’ -oxybis- 134 C6H14O3 000110-98-5 50 4 2-Pentanone, 5-methoxy­ 116 C6H12O2 017429-04-8 45 Abundance Scan 696 (11.432 min): 30353.D (-) m/z 59.05 100.00% 59

5000

-P 39. 45

+ 1-r-i-r 73 87 , 103

m/ Z _N 11.20 11.40 11.60 11.80 45.00 T-r-p-r

59.00%

1 m/z-> 30 40 50 60 70 80 90 100 110 120 130 Abundance #9238:2-Propanol, 1-(2-methoxy-1 -methylethoxy) 59

5000 TTTT • f ■ l • ■ • • l • • • ■ l ■ ■ • 45 103 11.20 11.40 11.60 11.80 73 31 m/z 103.00 33.76% --->1 1 1 1 1 i 1 r ......... ... 130 • > i > > miz-> 30 40 50 I60 70 80 90 100 110 120 130 Abundance -0086: 1-Propanol 2-12-hydroxypropoxy)- 59 *,**1****I**II‘‘I*V

NV 11.20 11.40 11.60 11.80 5000 m/z 73.00 27.21% 31 103 45 75 80 i ।■I।।।।‘i,।....j,,..।। । । । . j । । । . miz-> 30 40 50 60 70 80 90 100 110 120 130 Abundance #6087:2-Propanol, 1,1‘-oxybis- ’ 11 . . f. I . . . . I . . . . ( . i 59 11.20 11.40 11.60 11.80 m/z 41.05 26.79% 31

m/z-> 5000

- • j • ■ • * j i 30 40 45

1P+ 50 H 72 160 89 1 I 1 1 ' 1 1 1 1 ■ ■ i ■ • ■ ■ i 70 80 90 100 103

111 1 I 1 1 1 1 I 1 1 1 1 I 1 1 110 120 130 NA 11.20 11.40 11.60 11.80

30353.D GCMS1126.M Wed Jan 02 10:52:44 2002 Page 3

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