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GCMS analysis results for sample AD30352, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.

NYC-WTC_000017808–000017832

Folder label: “GCMS X 12/13/01 A 12/27/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30352.D Vial: 19 Acq On : 28 Dec 2001 5:38 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 16

R.T. EstConc Area Relative to ISTD R.T.

11.36 0.42 ug/1 134661 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 72 2 1-Propanol, 2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 59 3 2-Propanol, 1,1' -oxybis- 134 C6H14O3 000110-98-5 56 4 2-Propanol, 1,1'-[(1-methyl-1,2-eth 192 C9H20O4 001638-16-0 36 Abundance Scan 688 (11.357 min): 30352.D () m/z .00% 59 45 5000 73 103 ' i ■ ■ i • ■ ' ■ । ■ । ' । I । । । । I ।

miz-> —l 115150 ill60 70I'i't 30 40 iiii 80 ,84, 90 , 100 |............ 110 120 130 11.00 11.20 11.40 11.60 m/z 44.95 55.93% Abundance #9238:2-Propanol, 1-(2-methoxy-1-methylethoxy) 59

5000 45 103 Prii • i ■ • ■ ■ i 1 1 1 ■ i ' 11.00 11.20 11.40 11.60 73 31 m/z 103.05 32.46% 1 ■ 1 . . । I . . . । . i1 I ' 1 1 ' I 1 11 I I ‘ > I ■ I I > ‘ ■ I ‘I ■ 1 I 1 1 ‘ ‘ I"' T' 130 * | * > m/z-> 30 40 50 60 I 70 80 90 100 110 120 130 Abundance #6036: 1-Propanol. 2-(2-hydroxvpropo) 59 AAre T 11.00 11.20 11.40 11.60 T 18

5000 m/z 73.00 31.84% 31 45 103

m/z-> Abundance i

59 75 89 1 ' I ■ ‘ ‘ ■i•••■।।। i i ‘ ■ । ■ । ■ । । ■ ■ i i । • • ■ ■ । ■ ■ • • । • ■ । । ( ■ ■ 30 40 50 60 70 80 #6087:2-Propanol, 1,1-oxybis- 90 100 110 120 130 AMU 11.00 11.20 11.40 11.60 m/ z 41.05 27.14% 5000 31

• • । * * ‘ । । * 30 40 45

T5"7Hot 60 70 72 80 89 | 90 103

T t । । । । । । । । J » । ] i r 100 110 120 130 NA ' I ' ‘ ‘ 1 M I ‘ ' I ' ' ' ‘ I I I 1 I I f 11.00 11.20 11.40 11.60

30352.D GCMS1126.M Wed Jan 02 10:50:28 2002 Page 4

NYC-WTC_000017819

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NYC-WTC_000017819Source: NYC Law Department, mirrored locally

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