GCMS analysis results for sample AD30352, Jan 2002

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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.

NYC-WTC_000017808–000017832

Folder label: “GCMS X 12/13/01 A 12/27/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30352.D Vial: 19 Acq On : 28 Dec 2001 5:38 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclotetrasiloxane, octamethyl Concentration Rank 14

R.T. EstConc Area Relative to ISTD R.T.

11.13 0.48 ug/1 152710 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 86 2 Benzene, l-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 47 3 2-Oxo-4-phenyl-6-(4-chlorophenyl)-1 282 C16H11C1N2O 000000-00-0 9 4 1,3,5,7-Tetraethylbicyclo[3.3.1]tet 310 C8H2205Si4 073420-21-0 9 Abundance Scan 663 (11.128 min): 30352.D (-) m/z 281.00 100.00% 281

5000

■ ■ i 1 ‘ ■ i ■ ‘ 1 ■ i • • ■ ■ i 10.80 11.00 11.20 11.40

miz-> r 40 .. 45 59 ’ 80e i ’11 1 60 3,89 103n "V119I“>123 । i147r । . I163r I > .177,| . *1*113,207 IT r I ।'! 100 120 140 160 180 200 220 240 260 280 | . r. ..,. 235. | .2*h.’225, |.. . ., Per m/z 282.00 I****I 28.19% Abundance #41966: Cyclotetrasiloxane, octamethyl- 281

5000 /’II-111 ■ ■ i ■ ■ ■ ■ i 10.80 11.00 11.20 11.40 m/z 283.00 18.71% 73 133 163 177 191 207 k 235 249 265 ■•i•11■i•‘■■i■• | m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39843: Benzene. 1-phenyl-4-(2-cyano-2-phenyletheny!) 281

10.80 11.00 11.20 11.40 5000 m/z 192.90 12.60% onn 253 126 203 , 266 224 243 . . miz-> 40 ' 6o' 80 100 120 140 160 180 200 220 " 240 260 280 Abundance #39756:2-Oxo-4-phenyl-6-(4-chlorophenyl)-1,2-dihydropyrimi ■ ■ । ■ • ■ ■ । ■ ■ ■ ■ । ■ ■ ■ ■ । • ■ ■ ■ । 201 10.80 11.00 11.20 11.40 m/z 73.00 12,. 27%

miz-> 5000

80 102 100 123 141 ' ' i ' 1 ■ ■ i ■ ■ ■ ■ i 1 ' ■ ■ i'1 ■ • ■ i • 1 ■

40 60 120 175 • i ■ • • ■ i ■ ■ • ■ i ■ 140 160 180 204 ■111'1" ■ r* or* t *'* ■ ■ i" 11 f 200 220 247 240 260 280 A 10.80 11.00 11.20 11.40 2 30352.D GCMS1126.M Wed Jan 02 10:50:23 2002 Page 3

NYC-WTC_000017818

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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.

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