Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
NYC-WTC_000017703–000017723Folder label: “GCMS X 12/13/01 A 12/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C: \HPCHEM\ 1 \DATA\DEC2 701\30425.D Vial: 5 Acq On : 27 Dec 2001 3:04 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclotetrasiloxane, octamethyl Concentration Rank 10
R.T. EstConc Area Relative to ISTD R.T.
11.13 0.55 ug/1 169767 1,4-Dichlorobenzene-d4 11.68
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 50 2 Benzene, 1-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 50 3 2-Oxo-4-phenyl-6-(4-chlorophenyl)-1 282 C16H11C1N2O 000000-00-0 9 4 4-Amino-5-(4-acetylphenylazo)benzoE 281 C14H11N502 000000-00-0 9 Abundance Scan 663 (11.129 min): 30425.D (-) m/z 280.95 100.00% 281
5000 ________ 11*11’I’’ ■ ■ i ■ • ■ ■ i
45 59 73 89 103119 112 147 163 177 113207 , , 235 249 265, r 10.80 11.00 11.20 11.40 m/z 282.00 28.44% m/z~> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #72646: Cyclotetrasiloxane, octamethyl- 281
T-r-pr-rT-r-p-r 5000 10.80 11.00 11.20 11.40 265 m/z 283.00 19.45% . _ 73 133 45 59 | T11d’/b’2t11**—1’2t’01’1 177 193 297 235 . L ’’1-110-’11131’ 1-’1’111*11111111111183 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance 439643: Benzene. 1-phenyl-4-(2-cyano-2-phenyletheny!) 281
10.80 11.00 11.20 11.40 5000 m/z 192.90 12.57% . 253 126 22 7 268 ________________________________________203 | 224 240 h ’ 1’112310—3211139-0131’11’33111’’T’1211*1*1111-1T’11-11"’’11111113 miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39756:2-Oxo-4-phenyl-6-(4-chlorophenyl)-1,2-dihydropyrimi 281 10.80 1100 11.20 11.40 ' ‘ ' m/z 133.00 12.32% 5000
102 123 141.... 175 204 .... 247 ..... I 1 ■ i ■ ■ ■ ■ i ■ • ■ 1 i ■ 1 ■ ' i • ' 1 ‘ i miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 10.80 11.00 11.20 11.40
30425.D GCMS1126.M Wed Jan 02 11:03:46 2002 Page 2
NYC-WTC_000017711
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NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017833
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017724
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30426 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017808
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018470
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018492
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017675
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30251 conducted on January 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000017649
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Laboratory log recording extraction parameters and sample counts for environmental samples processed in December 2001.
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NYC-WTC_000017654
Document showing calibration results for GCMS analysis of volatile organic compounds on December 27, 2001.
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Laboratory report documenting gas chromatography-mass spectrometry reference material analysis conducted on December 31, 2001.
Filed in the same folder
NYC-WTC_000017663
Laboratory report documenting gas chromatography-mass spectrometry blank analysis conducted on December 27, 2001.
Filed in the same folder