Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
NYC-WTC_000018445–000018469Folder label: “GCMS X 12/18/01 A 12/30/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC2701\30643.D Vial: 59 Acq On : 30 Dec 2001 5:02 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclotetrasiloxane, octamethyl Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T.
11.13 2.83 ug/1 1402060 1,4-Dichlorobenzene-d4 11.67
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclotetrasiloxane, octamethyl- 296 C8H2404Si4 000556-67-2 86 2 6,7 -Benzo-phenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 9 3 Benzene, 1-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 9 4 2-Oxo-4-phenyl -6-(4-chlorophenyl)-1 282 C16H11C1N2O 000000-00-0 5 Abundance . Scan 663 (11.130 mln): 30643.D (-) m/z 281.00 100.00% 211
5000 -PPP » » ' j ' i I" l' >" J 45 59 73 89 103 119 133 147 163 177 123 207 221 235 249 285 [ 10.80 11.00 11.20 11.40 1I1C—TuummTutmfuTTTemaaTTTaT m/z 282.00 27.86% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 281
5000 ‘ I* ‘ 84 I 1-‘ l 1 * * • 1 10.80 11.00 11.20 11.40 m/z 283.00 17.66% .......... .................. .163 177.191 2 235 249 265. . m/z-> 40 60 80 100 120 140 160 180 200 220' 240 260' 280 Abundance #39602. 6,7-Benzo-phenothiazine-5,5-dioxide 281 1 • i ■ ■ • ■ i 10.80 11.00 11.20 11.40 5000 m/z 192.90 11.30% 217 232 ij 102 118 189 204 252264 1 * । •»• * ।» • i • ■ • • i * ‘ ‘ i • • • • i ■ • • • i • ■ • ■ i1 ■ ‘ • i1 • ‘ ''i * ■ 11611111111113 miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39643: Benzene, 1-phenyl-4-(2-cyano-2-phenylethenyl) 1 ■ i • ■ ■ • i ■ • 1 i ■ ■ ■ ■ i 2111 10.80 11.00 11.20 11.40 m/z 133.00 11.01% 5000 253 126 203 p i 266 ||
m/z—> 111 ■ ■ • ■ i1 • ■ ■ i • ■ • ■ i' • • • i ■ • • • i • • ■' i' "TT/l’l 11 ] 40 60 80 100 120 140 160 —2449444 180 200 220 240 260 280 ‘ ‘ I ’ ' * ‘ I ‘ 10.80 11.00 11.20 11.40 1 ■ i 1 ■ ' 1 i
30643.D GCMS1126.M Fri Feb 01 10:47:50 2002 Page 3
NYC-WTC_000018453
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NYC-WTC_000018470
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018492
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018519
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017808
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017833
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017724
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30426 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018416
Single-page document containing GCMS data or metadata associated with the WTC site in December 2001.
Filed in the same folder
NYC-WTC_000018417
Laboratory log sheet detailing Method 508 extraction and analysis parameters for samples processed in December 2001.
Filed in the same folder
NYC-WTC_000018420
Laboratory report documenting GCMS blank analysis of sample AD30643 conducted on February 1, 2002.
Filed in the same folder
NYC-WTC_000018436
Laboratory report documenting GCMS calibration data for sample AD30643 conducted on February 1, 2002.
Filed in the same folder
NYC-WTC_000018440
Laboratory report documenting GCMS reference analysis of sample AD30643 conducted on February 1, 2002.
Filed in the same folder