GC/MS calibration data for sample 30645, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC2701\30645.D Vial: 53 Acq On : 30 Dec 2001 10:14 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclotetrasiloxane, octamethyl Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

11.13 1.68 ug/1 688674 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclotetrasiloxane, octamethyl- 296 C8H2404Si4 000556-67-2 86 2 Benzene, 1-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 50 3 2-Oxo-4-phe: yl-6-(4-chlorophenyl)-1 282 C16H11C1N2O 000000-00-0 9 4 6,7-Benzo-p enothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 9 Abundance / Scan 663 (11.132 mln): 30645.D (-) m/z 281.00 100.00% 201

5000 I I I I < I < I I 11 I I < • ll I1’ s 1 I

45 59 73 89 103 119133 147 163 177 13 2^7 221 235 249 225 10.80 11.00 11.20 11.40 j । r’’er ( r’r j. I ri "Ir f’ ri’ j r’ | J r’ 1’r j T"T j rTi । TT Iasga H i । i I i > । Her m/z 282.00 28.19% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 281

Adgdsss188118*11 1 5000 10.80 11.00 11.20 11.40 m/z 283.00 17.25% 79 133 . 104 207 235 249 265 | ............. 7..................T........ 163 177 191 1 ■ i • ■ ■ 41 ■ ■ ■ • i • • • • i ■ ■ m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39643: Benzene, 1-phenyl-4-(2-cyano-2-phenyletheny!) 281 T I ‘ ‘ T TErCI 10.80 11.00 11.20 11.40 5000 m/z 192.90 11.77%

126 203 । 266 1 224 240 , k Pi ■ ■ । ■11 ■ i • ■ ■ • । ■' ■ • । • ■ ■ ■ । ■ • ■ • । ■ i ■ ■ ■ • । • ■' ■ ।1 ■ ■ ‘ i ■ ■ ■ • i •1 • • ।1 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 < I | > I TT । . > i ) >> i i | 1 I i i |

Abundance #39756:2-Oxo-4-phenyl-6-(4-chlorophenyl)-1,2-dihydropyrimi 231 10.80 11.00 11.20 11.40 m/z 133.00 10.77% 5000

102 123 141 175 204 247 —TI1—0n)—nnnuntpmnmnmnntonn—onnt—nunf I t I I I I » 18 ■ ■ i • • ■ ■ i m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 10.80 11.00 11.20 11.40

30645.D GCMS1126.M Fri Feb 01 10:52:37 2002 Page 3

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