GCMS analysis results for sample AD30351, Jan 2002

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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.

NYC-WTC_000017833–000017853

Folder label: “GCMS X 12/13/01 A 12/27/01”

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NYC 9/11 Public Portal Document . Library Search Compound Report

Data File : C: \HPCHEM\ 1 \DATA\DEC2 701\30351.D Vial: 20 Acq On : 28 Dec 2001 6:36 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclotetrasiloxane, octamethyl Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

11.13 0.69 ug/1 196289 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual l Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 80 2 Benzene, l-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 50 3 2-Oxo-4-phenyl-6-(4-chlorophenyl) -1 282 C16H11C1N2O 000000-00-0 9 4 6,7-Benzo-phenothiazine- 5,5-dioxide 281 C16H11NO2S 000000-00-0 9 Abundance Scan 663 (11.129 min): 30351 .D (-) m/z 281.M 100.00% 201

5000

’ * I * ' ‘ * I ‘ ‘ 1 * I r ‘ ‘ I ’ ‘ ‘ ‘ I 73 133 193 2 r 249 265 1 10.80 11.00 11.20 11.40 45 59 | 88 103 119, | 147 163 177 1l -Y 235 i., L HI, .I * , .’p I M I i T ri ITermgtri fT> i lu| rrt"i prt > i I I 1 ' ■ p • 1 ■ i ■" • ■ i T m/z 282.00 28.55% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #72646: Cyclotetrasiloxane, octamethyl- 2(11

5000 T A 10.80 11.00 11.20 11.40 265 m/z 283.00 17.20% 7 45 59 | 133 177 193 297 235 L 1***1’*I* ■ ■ i ■ • • ■ i ' ‘ ‘ • i ‘ ‘ i ‘ ■ 'V11144’414444141’41 14 । > p । miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39643; Benzene, 1 -phenyl-4-(2-cyano-2-phenyleteny‘) 281

10.80 11.00 11.20 11.40 5000 m/z 73.0,0 11.95% . 253 126 203 266 | 224 240 ; T miz-> Abundance ■ ‘ i ' ‘ ‘ ' i ■ ■ ■ • i ■ • 1 1 i' ‘ 40 60 80 100 ' i 120 111 140 160 180 200 #39756:2-Oxo-4-phenyl-6-(4-chlorophenyl)-1,2-dihydropyrimi 220 240 260 280 281 T

m/z 192.90 T 10.80 11.00 11.20 11.40 N. ‘ l ‘

11.88% * I

5000

........ 192 , J 23 t 141....... 175 204.......... 247 ........ Il 1 1 i 1 ■ 1 ■ i ■ ■ ■ ■ i 1 1 1 1 1 1 1 1 ' i miz-> 40 60 " 80 100 120 140 160 180 200 220 240 260 280 10.80 11.00 11.20 11.40

30351.D GCMS1126.M Wed Jan 02 10:46:02 2002 Page 2

NYC-WTC_000017841

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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.

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