NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2701\30351.D Vial: 20
Acq On : 28 Dec 2001 6:36 am Operator: 209 GALOS
Sample : GC/MS SCAN 12/13 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
14.31 2.59 ug/1 907962 Naphthalene-d8 15.28
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 56
2 Benzoic acid, 2,5-bis(trimethylsilo 370 C16H30O4S13 003618-20-0 43
3 Benzoic acid, 2,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 40
4 N-(Trifluoracetyl)-0,0*,0”-tris(tri 495 C20H36F3NO4Si3 000000-00-0 25
Abundance Scan 1009 (14.306 min): 30351.D (-) m/z 72.9.5 100.00%
73
5000
267
355
45 , J 88 103 133 154 177 193 223 251 , 293 323339 h 14.00 14.20 14.40 14.60
i
’ ’hT 1M1—mmETumum—nuTr . ।. 11 >.. f... .1., .... । m/z 267.00 33.95%
m/z~> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360
Abundance #51266: Cyclopentasiloxane, decamethyl-
73
355
267 ________ /__________
5000 • « l • • • • ) • • • T । , I r’ l j
| |
14.00 14.20 14.40 14.60
m/z 355.0 25.61%
191207 251 323339 j;
m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360
Abundance #73978: Benzoic acid, 2.5-bis(tnmethylsiloxy)- trimethyls
73
355
14.00 14.20 14.40 14.60
5000 m/z 267.90 9.61%
45
147 179 207223 267282297 370
mfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 17
Abundance #51296: Benzoic acid, 2,6-bis[(trimethyisilyl)oxy]-, trimet 1 ■ i • ■ • • i 1 • ■1 i 1 ' r 1 1 1 1 1 1 1
73 355 14.00 14.20 14.40 14.60
m/z 356.0. 9.23%
5000
147 267
.. .... ,... 208
47 249 1 ...... . 370
1’t5t1-1-1’-1111111011111___OI-T10201’119313093Im—O3I1STICWOOI3TTTTTTTT
T ’IITuri ■■ । ■1 i''1' i'11'।11 >11
m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.00 14.20 14.40 14.60
30351.D GCMS1126.M Wed Jan 02 10:46:07 2002 Page 3
NYC-WTC_000017842
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