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GC/MS calibration data for sample 28322, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.

NYC-WTC_000018492–000018518

Folder label: “GCMS X 12/18/01 A 12/30/01

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2 701\28322.D Vial: 62 Acq On : 30 Dec 2001 7:56 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Cyclopentasiloxane, decamethyl Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

14.31 10.09 ug/1 4732340 Naphthalene-d8 15.28

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 72 2 Benzoic acid, 2-[(trimethylsilyl)ox 282 C13H2203Si2 003789-85-3 38 3 N-(Trifluoracetyl)-0,0',0"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 37 4 Benzoic acid, 2,6-bis[(trimethylsil 370 C16H30O4S13 003782-85-2 33 Abundance Scan 1009 (14.308 min): 28322.D (-) m/ Z 73.0,0 100.00% 73

5000 267 355 V........ T T ' 7 I ‘ ‘ ‘ 1 1 • ‘ ‘J 45 108 133154 193 223 , 293 323 । 14.00 14.20 14.40 14.60 0- - TTI——T*dor—IT m/z 267.0,0 35.82% miz-> 50 100 150 200 250 300 350 400 450 500 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 * 1 । * ■ i < * * i i * * * » । * * » > । 14.00 14.20 14.40 14.60 m/z 355.05 27.72% I,............................ 207 | 323 j 1 1 I ' 1 1 ' i 1 1 ' ' 1 1 m/z-> 50 100 ' ' 150 ' '266 ' 250 300 350 400 450 500 Abundance #72208: Benzoic acid 2-[ttrmetnyisiMy K/ fr nathiysi 73 267 ‘ ‘ ‘ I ‘ ‘ ‘ ‘ I • ' • T I * 1 ' 1 I * 1 *' ‘"1 14.00 14.20 14.40 14.60 5000 m/z 356.05 10.12%

135 47 193 233 miz-> 50 100 150 200 ' 250 ' ' 300 350 400 ' ' 450 ' ‘ 500 Abundance #58807: N-(Trifluoracetyl)-O.O',O"-tris(trimethylsilyl)epin 14.00 14.20 14.40 14.60 355 m/z 268.00 9.42% 5000

45 I h T—r-|—i—r-> .. 140 184 .281 1 1*1—/——————480 / m/z~> 50 100 150 200 250 300 350 400 450 500 14.00 14.20 14.40 14.60/11

28322.D GCMS1126.M Wed Feb 06 12:55:58 2002 Page 5

NYC-WTC_000018502

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NYC-WTC_000018502Source: NYC Law Department, mirrored locally

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