GC/MS calibration data for sample 28322, Dec 2001

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\28322.D Vial: 62 Acq On : 30 Dec 2001 7:56 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Undecane, 4,6-dimethyl- Concentration Rank 20

R.T. EstConc Area Relative to ISTD R.T.

12.95 0.46 ug/1 179102 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Undecane, 4,6-dimethyl- 184 C13H28 017312-82-2 59 2 Decane, 2,6,6-trimethyl- 184 C13H28 062108-24-1 59 3 Hexane, 1-(hexyloxy)-5-methyl- 200 C13H280 074421-19-5 50 4 Undecane, 2,8-dimethyl- 184 C13H28 _ 017301-25-6 50 Abundance Scan 861 (12.949 min): 28322.D (-) m/z 57.00 100.00% 57

5000

m/z~> . .W J 43 71

85

I , „ 99 112....... 141 150............... m/z 71.05 ‘ I “1 12.60 12.80 13.00 13.20 ‘ ' 70.95% ।1111 44 । 1111 l'| n ■ 11 l'n r| i 1111 . . .. 11 11 i | > I I 11 i i 11 | 111 111 i > i । i 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 NA_ Abundance

5000

p| 98 113 57

71

141 #19008: Undecane, 4,6-dimethyl-

85 184 MN 12.60 12.80 13.00 13.20 1 m/z 43.05 59.68%

/VWJwr . i. • • > ।• i ■ ■ ■ ■ i ■ ■ ।11' •" .।j।t......... j।।. m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19023: Decane. 2,6,6-trimetry- 57

12.60 12.80 13.00 13.20 5000 43 m/z 56.00 51.02% 71 127 85 99 TI TMT i ‘ ■ ■ ■ i ■ ■ “ i ■ ■1 ■ i ■" ■ I ■ ■ ■' i1 ■" i ‘ “ ■ i ■ ■ ■11 l • ‘ • l ■ • • • l “ ■ ‘ I •' • • I Tr mfz~> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #23021: Hexane, 1-(hexyloxy)-5-methyl- ‘IStI4AII4/4.I * * I ’ 43 57 12.60 12.80 13.00 13.20 m/z 41.05 41.35% 5000

miz-> H 27 “ I 111,1 I U 70 85

• I * ‘ ‘4 f'1 "TITu • | n . । 97 115 11 j .Tt. 1’’’}**4’1’ 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 VW/Wn 12.60 12.80 13.00 13.20

28322.D GCMS1126.M Wed Feb 06 12:55:53 2002 Page 4

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