GCMS sample AE07106 analysis report with surrogate recovery, Apr 2002

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APRI8 02\7106.D Vial: 25 Acq On : 19 Apr 2002 11:38 am Operator: Sample : GC/MS SCAN 3/26 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS0419.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Undecane, 2,6-dimethyl- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

16.10 0.56 ug/1 132036 Naphthalene-d8 15.85

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Undecane, 2,6-dimethyl- 184 C13H28 017301-23-4(90 2 Dodecane, 6-methyl- 184 C13H28 006044-71-9 83 3 Undecane, 2,5-dimethyl- 184 C13H28 017301-22-3 64 4 Decane, 2,5,9-trimethyl- 184 C13H28 062108-22-9 64 Abundance Scan 1204 (16.097 min): 7106.D (-) m/z 57.00 100.00% 57

5000 43 71

98 F । I V i । i [ A iiii [ i T I I | I I

85 113 15.80 16.00 16.20 16.40

m/z-> .... .1, q I 4 I ++I rttl ' ।' 1111/1 I | I I I 137 I 151 | T 166 v 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Il 123 IFpTpd i'i I I I l'l I I I I I I I I I I I m/z 71.00 41.79% Abundance #69033: Undecane, 2,6-dimethyl- 57

5000 43 TBii । । ।' । | i r । i । । ii I । । ।

71 15.80 16.00 16.20 16.40 m/z 43.05 40.61% 85 98 113 .... I.....Tt TTTTTTTTTTTTTTTTTTTTTTT 140 184 | I i I I | ; i ■ I | 1 I T II‘1 i11 ■11'''' i ।11111' m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19006: Dodecane, 6-methyl- 57 — , — 51 15.80 16.00 16.20 16.40 5000 43 m/ Z 41.05 27.58% 71

85 98 112 mlz-> 30 i ■ ■ ■ ■ r 40 50 puljonnad 60 T."**nT 140 i ■1 ■11' ■ i ■1 ■11 70 80 90 100 110 120 130 140 150 160 170 180 190 184 ' i111111

Abundance #69031: Undecane, 2,5-dimethyl- 1 I |I—1—T1 [ I I I T I "I _I1 1 I I 57 15.80 16.00 16.20 16.40 m/z 98.05 18.35%

5000 71

m/z—> m 30 40 50 60 70 • i ■ 80 85 ’ i ' 1 99 112 TTIITT i1 ■ ■ ■ i 141 154 -0000001003033- 90 100 110 120 130 140 150 160 170 180 190 169 184 15.80 16.00 16.20 16.40

7106.D GCMS0419.M Mon Apr 22 08:34:03 2002 Page 7

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