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GCMS sample AE07106 analysis report with surrogate recovery, Apr 2002

Machine-extracted title · confidence 90%

Gas chromatography-mass spectrometry analysis report for sample AE07106 including surrogate compound recovery data.

NYC-WTC_000043458–000043471

Folder label: “GCMS X 4/23/02 A 4/24/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APR1802\7106.D Vial: 25 Acq On : 19 Apr 2002 11:38 am Operator: Sample : GC/MS SCAN 3/26 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0419.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Tridecane Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

17.66 0.66 ug/1 154311 Naphthalene-d8 15.85

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tridecane 184 C13H28 000629-50-5(98 2 Tetradecane 198 C14H30 000629-59-4 91 3 Eicosane 282 C20H42 000112-95-8 87 4 Dodecane 170 C12H26 000112-40-3 86 Abundance Scan 1374 (17.657 min): 7106.D (-) m/ z 57.00 100.00% 43 57

71 5000 85 J T ' i 1 1 184 17.40 17.60 17.80 18.00 99 113126 141 155 m/z 43.05 i m 1 *1ut Ti । । T । । 1 । i f i i rr । i r । ■ । 11 ■' । ■ ■ ■ ■ ।1 ■ ■ ■ । ■ ■ ■ ■ । > । •

4 80.83% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #18989: Tridecane 57 43

71 5000 85 i i । i i i i । i i i k i ! i r~। i r 17.40 17.60 17.80 18.00 m/ Z 71.00 57.30%

I 1 ' 11 I 1 1 12112 127 141.... 184 1 i n i । l i t i t il | ii rn ] i i i 1 । T 1 — I I I I j | | I I | I | | | | Illi j I I I — IT m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #69661: Tetradecane 57 43 71 17.40 17.60 17.80 18.00 5000 m/ Z 41.05 42.45% 85

m/z-> 27 | I. 99 113 155 198 i 1 1 1 | I I I | । । । । j i i r i । i । r । l । । । । । । । । । rn । । । i n r । ’i । i 111 i । । । । i i i । ’ । ( ! i ! 1 r 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #72323: Eicosane 43 57 17.40 17.60 17.80 18.00 m/ Z 85.05 37.78%

5000 71

85 4 . . 99 113 127 1 41 282 । i n i । i ,i t। ili । ,i i ill1 । । T i i 1 i i ti ] n । i [1 i i । | i । i । [ m । । । । । i । । । । i । । । । । । । । । । । । । । ......... 1 1 i ‘ ' 1 i ; 1 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 17.40 17.60 17.80 18.00

7106.D GCMS0419.M Mon Apr 22 08:34:03 2002 Page 8

NYC-WTC_000043470

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NYC-WTC_000043470Source: NYC Law Department, mirrored locally

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