TCLP calibration table review document, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\APR1202\8481.D Vial: 26 Acq On : 16 Apr 2002 9:08 am Operator: Sample : gc/ms scan 4/10 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 8 Tridecane Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 17.68 0.43 ug/1 84546 Naphthalene-d8 15.87 Hit# of 5 Tentative ID MW MolForm CAS# 9uad 1 Tridecane 184 C13H28 000629-50-5 93 1 2 Hexadecane 226 C16H34 000544-76-3 91 / 3 Heptadecane 240 C17H36 000629-78-7 91/ 4 Tetradecane 198 C14H30 000629-59-4 91 Abundance Scan 1376 (17.675 min): 8481 .D (-) m/ z 57.00 100.0CT%''' 57 43

71 5000 85 TPI 1 r ।' TT 0 । । i 7 17.40 17.60 17.80 18.00 99 113 126 141 184 -— — alg—a । । । i + 1 | । "i [ i p r i i i । i i i i । I i i i । i i i i । i i i i । i r m/z 43.05 80.31% mfe-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #18989: Tridecane 43 57

71 5000 85 TiT TTPPP 17.40 17.60 17.80 18.00 m/ z 71.10 56.81%

I’’ 11112 127 141..... । |i । । । i । । । । r~i i । । । । r । । । । । i l i-1 1 । r1 184 — I I I I I I I I I I I r 1r rr lz-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #70787: Hexadecane 43 57 p A AA of I | | | mM- N Tr 1 A 1 71 17.40 17.60 17.80 18.00 5000 m/ z 85.00 35.75% 85

27 99 113 127 141 155 226 I*’ 1 i 1 1 1 1 1 11 1 i । m&-> 20 40 60 80 100 120 140 160 180 ' 200 220 240 ,................. / A A Abundance #71191: Heptadecane 1 1 [ > 1 • ' | • 1 1 | li “i i f i i 57 17.40 17.60 17.80 18.00 43 m/z 41.05 35.44% 71 5000 85

— — I 99 113 127 141 | I I I I | T I A r I I r rl '( I I "I” I ............................. 240 1 I I 1 < I I I I ! I-1 I I Es I I I T mZz-> 20 40 (60 80 100 120 140 160 180 200 220 240 17.40 17.60 17.80 18.00

8481.D GCMS0412.M Fri Apr 26 12:47:27 2002 Page 8

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