GCMS analysis results for sample AE11309, May 28, 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\MAY2102\11308.D Vial: 22 Acq On : 21 May 2002 9:28 pm Operator: Sample : EXTRACTS/14 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 3 Heptadecane Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 19.29 0.77 ug/1 61465 Acenaphthene-dl0 21.08 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Heptadecane 240 C17H36 000629-78-7 2 Hexadecane 226 C16H34 000544-76-3 90 3 Tridecane 184 C13H28 000629-50-5 90 4 Tetradecane 198 C14H30 000629-59-4 86 Abundance Scan 1555 (19.288 min): 11308. D (-) m/z 57.10 100.00%! 43 57

71 5000

... J 85

9 99 113 '' ' 1 '' ' i ' ' ' 1 i ' ' ' 1 i ' 1 1 1 1 1 ‘ 1 1 i 1 1 1 ■ i 1 1 1 1 i ■ I m/ z 1 1 T1 1 L 19.00 19.20 19.40 19.60 43.10 83.30% m/z-> 20 40 (60 80 100 120 140 160 180 200 220 240 Abundance #71191: Heptadecane 57 43

71 5000 __ iA/ 1 ‘ 111■I 11■ 1 । ■ r 1 1 । 1 1 85 19.00 19.20 19.40 19.60 m/z 71.20 56.54%! anvaan—l+T" 99 113 127 141 240 m/z-> 20 40 160 80 100 120 140 160 180 200 220 240 Abundance #70787: Hexadecane 43 57 // 71 1 1 ■ i ' 1 1 1 i 1 ] 1 1 i ’ ' 1 1 i ' 1 19.00 19.20 19.40 19.60 5000 m/z 41.05 37.51% 85

27 , 1i ■ ' ■ 1 i 1 1 I ,l r 99 113 127 141 155 226 mlz-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #69019: Tridecane 43 57 19.00 19.20 19.40 19.60 m/z 85.15 29.13% 71 5000 85

m/z—> H 20 40 60 99 113 127 1 i 1 1 ' 1 । 80 100 184 ' 1 1 । ■ '1 ■ । ' • ‘ ' i ' ' : ' i ’ ■ ' ■ i ’ ■ ■1 । ■ ■ 1 ■ । ' 1 120 140 160 180 200 220 240 n Ar 1 i ' I’ 1 ' 1 1 1 1 19.00 19.20 19.40 19.60 -A—

11308.D GCMS0520.M Wed May 22 09:21:18 2002 Page 3

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