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GCMS analysis results for sample AE07490, April 2002

Machine-extracted title · confidence 100%

DEP laboratory report showing GCMS analysis results for sample AE07490 conducted on April 23, 2002.

NYC-WTC_000047137–000047146

Folder label: “GCMS X 4/1/02 A 4/20/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APR18O2\749O.D Vial: 23 Acq On : 20 Apr 2002 3:01 pm Operator: Sample : gc/ms scan 4/1 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0419.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Heptadecane Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 35.06 0.34 ug/1 44170 Chrysene-dl2 33.64 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptadecane 240 C17H36 000629-78- 7/87/ 2 Hexatriacontane 507 C36H74 000630-06- 8 87 3 Pentatriacontane 493 C35H72 000630-07-9 87 4 10-Methylnonadecane 282 C20H42 000000-00-0 87 Abundance Scan 3270 (35.063 min): 7490.D (-) m/ z 57.00 100.00% 43 57 71 /|

85 5000 m । MAA A MA,/ , A PWMMWP 97 —T 1 1 ' 1 1111 127 141....... 209 240 । । । m /“> — n i i | I i i i । i i i i r i r 281 m/z 34.80 35.00 35.20 35.40 43.05 85.74% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #71193: Heptadecane 57

5000 71 85 oovwl wooow 34.80 35.00 35.20 35.40 m/z71.10 83.03% 99 > J 113 127 141 155 169 210 240 1' ।' 1Bit i L ] I । T । | । i I i | । r i i | i i r < | i ' r" i i । i i i r | i i i i j i r i l | i i— i— i " । < i-1 " i । i i m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #74635: Hexatriacontane 43 57 . 1 . A A A ‘ ‘ ' 1 I ' 1 ' 1 | 1 1 1 1 | ’ I 111 ('1 v I 71 34.80 35.00 35.20 35.40 5000 85 m/z 85.05 57.27%

m/z-> 1 1 i 1 ' 40 11.87 113127 141 155 180 196200210220225 239 11 ‘' ■111'' 'i1111।'''11' 1 ■11 ’ 60 80 100 120 140 253 267 281 240 260 280160 1III1’*** Abundance 43 57 #58743: Pentatriacontane —AA AA I 1 ' 1 ' 1 34.80 35.00 35.20 35.40 rn/z 41.05 34.09% 71 5000 85

97

m/z-> U60 80 100|,| 113120127 140 1 ■ i 1 40 141 155 169 183 197 211 225 239 ■ ‘I । i r 1 [ । । । 1 । । । 160 180 200 220 240 260 280 AAAAA 34.80 35.00 35.20 35.40

7490.D GCMS0419.M Mon Apr 22 12:36:24 2002 Page 2

NYC-WTC_000047145

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NYC-WTC_000047145Source: NYC Law Department, mirrored locally

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