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GC/MS analysis results for sample AD23799, Nov 1 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23799 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089311–000089332

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089328
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C;\HPCHEM\1\DATA\OCT3001\23799.D Vial; 10 Acq On : 30 Oct 2001 11:19 pm Operator: 209 GALOS Sample ; gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title ; 209 625/TCLP calibration table Libraary : C;\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 Heptadecane, 8-methyl- Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T. 34.56 0.94 ug/1 267367 Chrysene-dl2 33.06 Hit# of 5 Tentative ID MW MolForm CAS# Qua

1 Heptadecane, 8-methyl- 254 C18H38 013287-23-5(93 2 Hexatriacontane 507 C36H74 000630-06-8 91 3 Octacosane 394 C28H58 000630-02-491 4 Heneicosane 296 C21H44 _______ 000629-94-7 91 Abundance Scan 3215 (34.556 min); 23799.D (-) "m/z 57700 100.00% 57

85 5000 4' 34.20 34.40 34.60 34.80 J 169 196211 239255 ' I ip I l■‘f| inrfTi if) I i-fi I ft I I-fl I lA I I fl I I n 11 ri ri'i I I 11 p-rrq-i n 11 111 i । 111 i i-i'i i 11 i i m/z 71705 71.28% Tife-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #34816: Heptadecane, 8-methyl- 57

85 5000 FT 34.20 34.40 34.60 34.80 126 m/z 43.05 67.52%

Ti/iz-> Abundance XUxL Or 154

40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 224 254 ' I'''' I'''' I I•"'I '•" I’" ' r " 'I

___ _#74636: Hexatriacontane --------------------- ---------------- 57 I i^i j I I I 'I I 1^^ 7 'in r I

34.20 34.40 34.60 34.80 5000 85 m/z85.0557.05%

_XjL21Lx1dIl69197_______ __ ___________ " I'' yrVYTyTTTT“p-rTTpVrq^rTTVpn"TTp-rrTpTT-TYrTTTp-rTTyTTrrpTTTyrT^^ Tife-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #74211: Octacosane -4 ■-■34.20-.34.40-34 60 - 34.80-^— “m/z 41.05 26717% 71 5000

\ 1 , 127 155 183 211 364 - I.... |Ti. 11.1 / i I.... I..I. I'l. I’l I, I'l.. I' I' > I • 1111" I ■ I •' I • 11 > •' ■nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 34.20 34.40 34.60 34.80

23799.D NP103001.M Thu Nov 01 13:16:57 2001 Page 11

NYC-WTC_000089328

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NYC-WTC_000089328Source: NYC Law Department, mirrored locally

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