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GC/MS analysis results for sample AD23838, Nov 2 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23838 conducted on November 2, 2001, identifying unknown compounds.

NYC-WTC_000089346–000089365

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089362
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT3001\23838.D Vial: 12 Acq On : 31 Oct 2001 1:15 am Operator: 209 GALOS Sample : gc/ms, unknown Inst ; GC/MS 209 Mise Multiplr; 1.00 MS Integration Params; LSCINT.P

Quant Method : C;\HPCHEM\1\METHODS\NP101901 .M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C;\DATABASE\NBS75K.L ********************** * * *********************************'^*'A'********* Peak Number 10 Hexadecane Concentration Rank 4 R.T. EstConc Area Relative to IStD R.T. 33.63 20.00 ug/1 134484 Chrysene-dl2 33.39 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexadecane 226 C16H34 000544-76-3 93 2 Heptadecane 240 C17H36 000629-78-7 9^ 3 Hexatriacontane 507 C36H74 000630-06-8 91 4 Heptacosane ____________________ 380 C27H56 000593-49-7 87 Abundance Scan 3114 (33.629 min): 23838.D (-) m/z 5^700 100.00% 57

43 71 85 5000 _ _ v_ - | i-FFi-rrr I-I I I I-I IT I r . m 113 33.20 33.40 33.60 33.80 34.00

T)Zz-> 40 I,. JI80,I.. 100 'i:k) 140 160 180 200 60 240 ???,.,, 260 2^ “mTz 43705 65.65% Abundance #70790; Hexadecane 43

71 5000 85 33.20 33.40 33.60 33.80 34.00 Wz 71.10 65.52% ., j'... i',,, I,, .'I,, ...... 226 TTfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #71194: Heptadecane 4S-57-

71 I I I 33.20 33.40 33.60 33.80 34.00 5000 “iiiTz 85.05 51.52% 85

4=^ 27-141,155-169.183- -212 ' • I ■ ' ' ■ I ' ' • ' f' ' ' I ' ' I ' I ' ' ' ' __24O------- Tiy^-> Abundance — 40 60 _ 80 100 120 140 160 180 200 220 240 260 280 _ —43 - 5l7 ----- - #74636: Hexatriacontane E I ' ' 33:20 33.40 - 33.60 -33.80 34.00- - -m/z—41—05--- 27\7m 71 5000 85

1 971,1 prT-T-ryT-rT’T’Y^-T^HTVTT-q'-Tn-T-TTT-T-TT-p-Tir-ryT-T-^^ 197 211 ______ . ■n^-> 60 80 100 120 140 160 180 200 220 240 260 280 33.20 33.40 33.60 33.80 34.00

23838.D NP103001.M Thu Nov 01 14:33:49 2001 Page 10

NYC-WTC_000089362

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NYC-WTC_000089362Source: NYC Law Department, mirrored locally

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