GCMS analysis comments for sample AD28693, Dec 2001

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Library Search Compound Report Data File : C:\HPCHEM\l\DATA\DEC0401\28693.D Vial: 8 Acq On : 4 Dec 2001 7:12 pm Operator: 209 GALOS Sample : gc/ms 11/24 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Hexadecane Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 30.63 0.81 ug/1 156363 Chrysene-dl2 33.03 Hit# Of 5 Tentative ID MW MolForm CAS# Qu 1 Hexadecane 226 C16H34 000544-76-3 91 2 Heptadecane 240 C17H36 000629-78-7(91 3 Heptadecane, 2,6,10,15-tetramethyl- 296 C21H44 054833-48-6 91 4 Tetracosane 338 C24H50 000646-31-1 90 Abundance Scan 2787 (30,628 min): 28693.D (-) m/z 57.00 100.00% 57 43 71

5000 85

99 30.20 30,40 30.60 30.80 31.00

m/z-> — 40 60 1480 "1Tdu 1 113 127‘141 155 169 ‘183 ku—uuhu 197 211 "uurutT 253 100 120 140 160 180 200 220 240 260 280 300 m/z43.05 78.77% Abundance #70790: Hexadecane 43 57

71 5000 ====1--==-============ 85 30.20 30.40 30.60 30.80 31.00 m/z71.00 73.47%

m/z-> 1 — 1 — 113127 141 155 ........... ................. . , 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #71193: Heptadecane 57 -21 -P -A — ' ■ 71 30,20 30,40 30,60 30,80 31.00 5000 m/z 85.05 49.28% 85

99

nfe-> . A, 1 3127 141 155 ........ 210 ............... ' 1 I I • । । | >T 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #42196: Heptadecane, 2,6,10,1 5-tetramethyl- PPAT in i-| । ।-r > | । TPrfri 57 30.20 30.40 30.60 30.80 31.00 71 m/z 41.05 29.94% 5000 85

m/z—> ■11 •1 40 — 60 80 x 113127 .. 100 141 155 —183— 211 ... ...... 296 MMMYMPYYP 120 140 160 180 200 220 240 260 280 300 30.20 30.40 30.60 30.80 31.00

28693.D GCMS1126.M Thu Dec 06 15:19:41 2001 Page 4

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