GCMS analysis comments for sample AD28693, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC0401\28693.D vial: 8 Acq On : 4 Dec 2001 7:12 pm Operator: 209 GALOS Sample : gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclohexadecane Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 29.68 0.83 ug/1 160636 Chrysene-dl2 33.03 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclohexadecane 224 C16H32 000295-65-8 2 1-Heptadecanol, acetate 298 C19H38O2 000822-20-8 3 Acetic acid, octadecyl ester 312 C20H40O2 000822-23-1 90 4 3-Hexadecene, (Z) -__________ ' 224 C16H32 034303-81-6 83 Abundance Scan 2684 (29.682 min): 28693.D (-) m/z 100.00% 43

5000 57 70 83 97 111 AUU. T-r-j-rr

mlz-> TIT r 40 60 Ail.L2,14015480 100 192 207 224 p-rti-T 252 TH. T TT 11 f ITT -1J i'' • I ■ 120 140 160 180 200 220 240 260 280 300 m/z 29.40 29.60 29.80 30 00__ 55.00 51.34% Abundance #28780: Cyclohexadecane 55 83 69 97 - — r 5000 TTT 29.40 29.60 29.80 30.00 111 42 m/z 57.00 45.52% 125

mlz—> ■ > > । ■ < LC i ■ 1 ■ ■ i 11 11 ■1 1 ■ i ■ ■1 40 60 80 100 120 140 160 180 200 220 240 260 280 300 196___ 224 i ■ > ■ ■ i ■ > ■ ■ । > i • • ■ ■ i ■ ■ • • i ■ • ■ ■ i ■

Abundance #42500:1-Heptadecanol, acetate 43 — 83 29.40 29.60 29.80 30.00 5000 61 97 m/z 83.05 44.70% 111 125 .. 210 238

mz-> TII 1,14 i ■ ’ ■ ■ i I I 298 40 60 80 100 120 140 160 180 200 220 240 260 280 300 ■ l > • ' ■ i ■ ■ ■ • । ■ ■ ■ ■ । ■ i ■ ।■ i ■ ■ • ■ i ■ ■ ■ ■ । ■

Abundance #73048: Acetic acid, octadecyl ester - ------PI ।P 43 29.40 29.60 29.80 30.00

5000 83 97 m/z n 97.05 44.09%

61 111 42 m/z—> T-rp-r 40 L 14.4139 .. ... ........ 60 80 100 120 140 160 180 200 220 240 260 280 300 29.40 29.60 29.80 30.00

28693.D GCMS1126.M Thu Dec 06 15:19:39 2001 Page 3

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