GCMS analysis comments for sample AD28694, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\l\DATA\DEC0401\28694.D Vial: 5 Acq On 4 Dec 2001 4:16 pm Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1-Hexadecanol, acetate Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 29.68 • 0.61 ug/1 149937 Chrysene-dl2 33.04 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-Hexadecanol, acetate 2 Octadecanol 3 Acetic acid, octadecyl ester 284 C18H3602 270 C18H380 312 C20H40O21 000629-70-9 026762-44-7 000822-23-1 68 Q 4 1-Octadecanol 270 C18H380 000112-92-5 62 Abundance Scan 2684 (29.682 min): 28694.D (-) m/z 43.05 100.00% 43

83 5000 55 69 97 111 125 29.40 29.60 29.80 30.00

mlz-> — 40 J 111 60 4——1 80 4—4139.153... 207224 .. 100 120 140 160 180 200 220 240 m/z ,83.05 53.13% Abundance #40196:1-Hexadecanol, acetate 43

5000 61 83 97 111 — L A _A 29.40 29.60 29.80 30.00 m/z 55.00 48.81% 125 196 224 rtfz-> 1 1 I' ' 40 I ■ 1 ■ 1 I 60 80 —l100. I 139 154 " ' .............. TT T 11 । .... । I 120 140 160 180 200 220 240 । ,

Abundance #37846: Octadecanol 69 83 97 , , —A A 29.40 29.60 29.80 30.00 5000 56 111 m/z 60.95 46.90% 125 180 196 224 252 T-r-p-r i ■ ■ ■ ■ 1 1 < 1 i ’ • • • < i • • » i • • • TT m/z—> 40 60 80 100 120 140 160 180 200 220 240 Abundance #73048: Acetic acid, octadecyl ester — 43 29.40 29.60 29.80 30.00 m/z 69:00 45.80% 5000 61 83 97 111 — 125 139 224 252 TTTTTTTT 1 ' I1 1 ' i ' ' ■ ■ i ■ ■ ■ ■ i ■ ' 1 1 1 1 ‘ ' 1 P ■ ■ ■ i ■ ' ■ ■ i • ' ■ ■ i m/z—> 40 60 80 100 -120 140 160 180 200 220 240 29.40 29.60 29.80 30.00

28694.D GCMS1126.M Thu Dec 06 15:34:02 2001 Page 3

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