GCMS analysis results for sample AD28430, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\l\DATA\DEC0401\28430.D vial: 12 Acq On 4 Dec 2001 11:06 pm Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1-Heptadecanol, acetate Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 29.68 1.00 ug/1 249815 Chrysene-dl2 33.04 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Heptadecanol, acetate 298 C19H38O2 000822-20-8(91/ 2 3-Hexadecene, (Z) - 224 C16H32 034303-81-6 83 3 1-Nonadecanol 284 C19H40O 001454-84-8 81 4 Phosphonic acid, dioctadecyl ester 587 C36H7503P 019047-85-9 70 Abundance Scan 2684 (29.681 min): 28430.D (-) m/z 43.00 100.00% 43

61 83 97 5000 111 | 125 WA. 29.40 29.60 29.80 30.00 - . , I 139153 168 । 207 224 M r'1 '............ rpt.. ...... 252 m/z 55.00 51.79% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #42500:1-Heptadecanol, acetate 43

83 5000 61 97 29.40 29.60 29.80 30.00 111 m/z 60.95 49.51%

m/z—> ■ ■ i ■ ■ 40 60 117510 210 I__ | 238 I 1 ■ > 111 • • ■ i1 • ■ ■ । ■ 80 100 120 140 160 180 200 220 240 260 280 300 i ■ ■ ■ ■ i 298 1 ' 11

Abundance #28772: 3-Hexadecene, (Z)-

5000 55 69 | 83 97 —A. . 29.40 29.60 29.80 30.00 m/z 83.00 48.71% 42 111 | 125 11 r1' i' L 1 I— 196 224 ' i ■' ■ ' i ■ ■ ■ ■ i ■ ■ ■ ’ I' 11' 11TTT । 111 111 111 11 ■ > 111 miz—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #40236:1-Nonadecanol ----- 55 69 83 29.40 29.60 29.80 30.00 97 m/z 57.00 46.20% 5000 111 42

Xu 125

m/z—> 40 1 ‘II n-rr 60 80 238_________ 1I‘‘‘111111111011—TTrT‘*10rIu""I0"TITgT 100 120 140 160 180 200 220 240 260 280 300 AWA 29.40 29.60 29.80 30.00

28430.D GCMS1126.M Wed Dec 05 08:19:38 2001 Page 3

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