GCMS analysis results for sample AD28471, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\DEC0401\28471.D Vial: 7 Acc On 4 Dec 2001 6:13 pm Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1-Nonadecanol Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T. 29.69 0.89 ug/1 234827 Chrysene-dl2 33.04 Hit# of 5 Tentative ID MW MolForm CAS# Qual

l 1-Nonadecanol 284 C19H40O 001454-84-8 3 2 Acetic acid, octadecyl ester 312 C20H40O2 000822-23-1 3 1-Heptadecanol, acetate 298 C19H38O2 000822-20-8 90 4 Phosphonic acid, dioctadecyl ester 587 C36H7503P 019047-85-9 89 Abundance Scan 2684 (29.686 min): 28471 .D (-) m/ z 43.05 100.00% 43

83 69 97 5000

I 56 111 ___________

mz-> ll 40 60 80 125 139153 168 — TIIP1] 224 252 .......... ... ................................ I' 100 120 140 160 180 200 220 240 260 280 300 29,40 29.60 29.80 30.00 m/z 83.05 60.82% Abundance #40236: 1-Nonadecanol 55 83 69 97

5000 111 —4 29.40 29.60 29.80 30.00 42 125 m/z 55.00 52.43%

mlz-> I 40 X 100I 120 140 160 180 200 220 238 240 260 280 300 Abundance #73048: Acetic acid, octadecyl ester 43 —A .29.40 A..... — 29.60 29.80 30.00 5000 m/z 97.05 52.14% 83 97 61 111 — .. .............................. ................... ............................................

m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #42500: 1-Heptadecanol, acetate 43 29.40 29.60 29.80 30.00 m/z 69.00 50.30% 83 5000 61 97

Mi 111 i 125 210 238 140 ■ ■ AA - | — r " T’iTI’ r ' ■ ' i ■ ■ ■ ■ i ■ ■ ■' i' ' ' ■ i ' '1 ' i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ | | 298 miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29,40 29.60 29.80 30.00

28471 . D GCMS1126 .M Wed Dec 05 11:27:33 2001 Page 3

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