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GC/MS analysis report for sample AD22545, September 2001

Machine-extracted title · confidence 95%

Laboratory results for sample AD22545 indicating other unknown compounds detected via GC/MS on September 27, 2001.

NYC-WTC_000086933–000086948

Folder label: “508 Scan 9/17/01 9/26/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C;\HPCHEM\l\DATA\SEP2501\22545. D Vial: 11 Acq On : 26 Sep 2001 12:15 am Operator: 209 GALOS Sample : GC/MS unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DAT7kBASE\NBS75K.L ********************************************************************* Peak Number 5 Acetic acid, octadecyl ester Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 29.78 1.23 ug/1 162868 Chrysene-dl2 33.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, octadecyl ester 312 C20H40O2: 000822-23-1 87- 2 1-Heptadecanol, acetate 298 C19H38O2; 000822-20-8 86 3 1-Nonadecanol 284 C19H40O 001454-84-8 76 4 1-Pentadecanol 228 C15H32O 000629-76-5 74 Abundance Scan 2695 (29.780 min): 22545.D (-) m/z 43.05 100.00% 43 I 5000

*T

■nZz-> 40 JUXLu?’?”* 60 80 100 120 140 160 180 200 220 240 260 280 300 224 I'''' I ‘' I 252 29 40 29,60 29,80 30,00 30,20 m/z 60.95 57.76% Abundance #44575: Acetic acid, octadecyl ester 57 83 97 5000 70 T 111 29,40 29.60 29,80 30,00 30,20 m/z 83.05 56.64%

MI1 125 208 224 252 . I . . I . J . . ,4-r. . I 282 ' ' ' ' 1 ' ' ' 1 ' ' ' H ' I''' ' I ■nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #42500:1-Heptadecanol, acetate 43 n 83 29,40 29,60 29,80 30,00 30,20 5000 61 97 m/z55.00 51.78%

tVz->40 Abundance 60 m IX 80 111 I 125 140

100 120 -4- 210 1 238 I ' ' ' ' I ' ' ' ' I ' 140 160 180 200 220 240 260 280 300 #40236:1-Nonadecanol 298

55 83 29 40 29,60 29,80 30,00 30,20 I 69 m/z 97705 48.58% 97

5000 111 42 125

■nfe-> I I 40 JU V I 60 80 100 120 I ' ' ‘ ' I ' ' ' ' I ' ' ' ' I ' ' ' ' 1 140 160 180 200 220 240 260 280 300 238 ' I''' ' r , , , , , ,A, .............. .

29,40 29,60 29,80 30,00 30,20

22545.D NP091101.M Wed Oct 03 15:09:36 2001 Page 5

NYC-WTC_000086945

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NYC-WTC_000086945Source: NYC Law Department, mirrored locally

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