GC/MS analysis report for sample AD22545, September 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\SEP2501\22545.D Vial; 11 Acq On : 26 Sep 2001 12:15 am Operator: 2 09 G7VLOS Sample : GC/MS unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C;\HPCHEM\1\METHODS\NP091101 .M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C;\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Phosphonic acid, dioctadecyl e Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 31.90 0,48 ug/1 63160 Chrysene-dl2 33.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual CZ^Phosphonic acid, dioctadecyl ester 587 C36H75O3P 019047-85-9 92 2 1-Eicosanol 298 C20H42O 000629-96-9 81 3 Acetic acid, octadecyl ester 312 C20H40O2 000822-23-1 80 4 1-Octadecanol 270 C18H38O 000112-92-5 68 ^bundance Scan 2926 (31.900 min): 22545.D (-) m/z 43.05 100.00% 43

61 83 5000 97

JU L T 207 31,60 31,80 32,00 32,20 “m/z 60795 58.05% Abundance 40 60 80 100 120 140 160 180 200 #60683: Phosphonic acid, dioctadecyl ester 220 240 260 280 J 43 97

5000 111 J -pt-r 31.60 31,80 32.00 32,20 136 m/z83.05 57.66%

■n/z-> ' 40 UMUU 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #72722:1-Eicosanol 57 83 . r . I 1^ V I I . I I I I 69 97 31,60 31,80 32,00 32,20 5000 111 m/z 69710 54.54% 125 139 1R7

■n/z-> 40 UM J.. 167 ............... 2^ 100 120 140 160 180 200 220 240 260 280 Abundance #73048: Acetic acid, octadecyl ester I A A 43 31,60 31,80 32,00 32,20 m/z 54795 54.32%

5000 83 97 61 111

■nfe-> 40 bU |l t 60 80 100 120 140 ...... 160 180 200 220 ^^2... 240 260 280 31,60 31,80 32,00 32,20

22545.D NP091101.M Wed Oct 03 15:09:38 2001 Page 6

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