GCMS blank analysis results for sample AE09447, May 2002

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GCMS blank analysis report for sample AE09447 listing compounds below detection limits from May 8, 2002.

NYC-WTC_000045400–000045410

Folder label: “GCMS X 5/3/02 A 5/8/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\MAY0802\LB.D vial: 3 Acq On 8 May 2002 11:33 am Operator: Sample GC/MS SCAN 5/3 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0507.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L * * * * * * * ************************************************************** Peak Number 4 Phosphonic acid, dioctadecyl e Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

31.16 6.84 ug/1 322752 Chrysene-dl2 33.64

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phosphonic acid, dioctadecyl ester 587 C36H75O3P 019047-85-9 76 2 1-Octadecanol 270 C18H380 000112-92-5 76 3 5-Eicosene, (E)- 280 C20H40 074685-30-6 76 4 1-Heptadecene 238 C17H34 006765-39-5 68 Abundance Scan 2851 (31.163 min): LB.D (-) m/z 55.10 100.00% 55 A 43 5000 73 97 TI 171 T 1II 85 111 127 30.80 31.00 31.20 31.40 11U _ , J |1 141153 169 I I ' < ■ I I I I " I I i I I II I I [ ‘ I I I I I I I I I I ( 207 225 295 m/ z 43.10 58.41% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #60683: Phosphonic acid, dioctadecyl ester 55 69 83 43 97

5000 1 । 1 । । r I I nI i ] 1 i । । [ i i n [ r 30.80 31.00 31.20 31.40 111 136 m/z 57.10 49.25%

■11 ■ ■ TIn ■n-p- . ............................................................................ 1 । i i i i । i I । । । I i 1 i । i i । i । i i । i । । i i i ] I i i i [ i i i । । i 1 । t [ i n i |T mz- > 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #72029:1-Octadecanol 43 55 69 83 97 ------ TRMi 30.80 31.00 31.20 31.40 5000 m/ Z 73.10 45.30% 111 125 1 1 I1 ' TTT ""1 X | 224 252 m/z-> Abundance 40 60

55 80 100 120 140 160 180 200 220 240 260 280 300 #39520:5-Eicosene, (E)- A 1 > I ! । । > 1 30.80 31.00 31.20 31.40 | | I 1 | | r

m/z 83.15 43.37% 83 5000 97 70 111 , 125, 1l,.,1139... 252 280.. । ■ i ■ ■ i ' 1 ‘ 1 1 1 1 1 ■ 1 1 i 1 1 r ' i 1 1 1 1 i ’ 1 1 1 1 1 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 30.80 31.00 31.20 31.40

LB.D GCMS0507.M Thu May 09 14:43:53 2002 Page 4

NYC-WTC_000045409

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NYC-WTC_000045409Source: NYC Law Department, mirrored locally

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