GCMS blank analysis results for sample AE09447, May 2002

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GCMS blank analysis report for sample AE09447 listing compounds below detection limits from May 8, 2002.

NYC-WTC_000045400–000045410

Folder label: “GCMS X 5/3/02 A 5/8/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\MAY0 8 02\LB.D Vial: 3 Acq On 8 May 2002 11:33 am Operator: Sample GC/MS SCAN 5/3 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0507.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Anthracene-dlO- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

25.71 0.46 ug/1 38518 Phenanthrene-dl0 25.57

Hit# of 5 Tentative ID MW MolForm CAS# Qu.

1 Anthracene-diO- / 1 188 C14D10 001719-06-8 /90 2 Phenanthrene -diO 188 C14D10 001517-22-2/ 90 3 2-Quinolinecarboxaldehyde, 8-hydrox 188 C10H8N2O2 005603-22 -540 4 4H-Pyripo[1,2-a]pyrimidin-4-one, 3- 188 C11H12N2O 057773-19-0 40 Abundance Scan 2256 (25.710 min): LB.D (-) m/z 188.15 100.00% 188

5000

94 80 25.40 25.60 25.80 26.00 1 66 158

m/z-> 40 52 TTjT-rrq-TT -T-TT TTHTTTTTTTTTTTTTTTTTTTTTT 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 -HH m/ z 94.10 16.93% Abundance #19957: Anthracene-d10- 188

5000 T-n-r-r^Y^_r-r-rTT-r-TT-|-rT-T-T^ 25,40 25.60 25.80 26.00 m/ z 80.10 16.44% 66 80 34 .11° || > । । । । । । । । । । । । > । n In n n । | > । . । । I I । । । । i > । i । n | 1 1 1 ■ . 1 n 1 | 1 1 1 1 | ' 1 H n - I 1 i 1 | .' 111 I 1 । । r m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 188 ‘4//"B/UT1111tLIII/III 25.40 25.60 25.80 26.00 5000 m/z 189.15 15.23%

80 94 160 66 1 , I I I | | | i | [ | | | . | 11111 L . i , r n/z-> 30 40 50 — 60 70 80 H I'111 r 1'' r 1111 90 100 110 120 130 140 150 160 170 180 190 Abundance #69165: 2-Quinolinecarboxaldehyde, 8-hydroxy-, oxime ............ /.................................. 188 25,40 25.60 25.80 26.00 m/z 184.15 11.29%

5000

143 64 T 116 130 ...11 ■... 11... ।. | < I I I I I I j l mp III I I I I I I I I I I I I I I I I t I I I “1“ I I r I I o r I I 'l I I I I ill 158 179 rrr mfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00

LB.D GCMS0507.M Thu May 09 14:43:52 2002 Page 3

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