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GCMS analysis results for sample AE10159, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE10159 conducted on May 10, 2002.

NYC-WTC_000044804–000044814

Folder label: “GCMS X 4/29/02 A 5/3/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\1\DATA\MAY0 6 02\10159.D Vial: 7 Acq On 7 May 2002 11:42 pm Operator: Sample GC/MS SCAN 4/29 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0507.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Anthracene-dlO- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

25.71 0.46 ug/1 41163 Phenanthrene-dl0 25.57

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-diO- 5 188 C14D10 001719-06-8 72 2 Phenanthrene-diO 188 C14D10 001517-22-2 45 3 4H-Pyrido[1,2-a]pyrimidin-4-one, 3- 188 C11H12N2O 057773-19-0 38 4 2-Quinqlinecarboxaldehyde, 8-hydrox 188 C10H8N2O2 005603-22-5 9 Abundance Scan 2256 (25.711 min): 10159.D (-) m/z 188.15 100.00% 1(18

5000 — 80 94 25.40 25.60 25.80 26.00 40i" IITT54 . ।66 . 1. ।. + t 156 i ■ ■11 r 111 r '11 r 1'111 ■'' 11 ‘'1 r 1 I > | ! h I | i TT m/ z 80.05 20.98% m/z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 188

1 I | l t — | I ! I I | I I I I | I I I I r 5000 25.40 25.60 25.80 26.00 m/z 94.10 20.27% 80 94 160 । 66 ■ I'11' l1' ■ ■,1' 111 ■'' I. । ............ । |.... i j i i i i । i i i i p i i i j i i i i j ( i i i j > r i i j i i i i j i i i i । i n i p i < i p i i |l. | i i r i

m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 188 4 25.40 25.60 25.80 26.00 5000 m/z 189.15 16.07%

80 94 160 66 m/z-> 1PTT 40 50 60 70 80 — i'' ■ ■ i'1111 ■ ■'' i 4.— 90 100 110 120 130 140 150 160 170 180 190 ...... W... Abundance #19873: 4H-Pyrido[1,2-a]pyrimidin-4-one, 3-ethyl-6-methyl- 145 188 25.40 25.60 25.80 26.00 173 m/z 184.15 11.84%

5000 92

65 159 T n i i i P i i i | r I I i | I r 1 11''' ’ I | D9 132 1 ' ' I 1 i I 1 I 1 I ' l P l . I I I 1 1 1 I I ' । n 111 m । । I 4— 110 | ‘ I1*1*11111171/4/1/1+/1IL.I.1 m/z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00

10159 .D GCMS0507.M Thu May 09 11:12:14 2002 Page 3

NYC-WTC_000044813

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NYC-WTC_000044813Source: NYC Law Department, mirrored locally

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