GCMS analysis results for sample AE10159, May 2002

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Laboratory report documenting GCMS analysis of sample AE10159 conducted on May 10, 2002.

NYC-WTC_000044804–000044814

Folder label: “GCMS X 4/29/02 A 5/3/02”

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NYC 9/11 Public Portal Document

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Data File C:\HPCHEM\l\DATA\MAY0602\10159.D Vial: 7 Acq On 7 May 2002 11:42 pm Operator: Sample GC/MS SCAN 4/29 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0507.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 5-Hexen-2-one Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

9.97 0.60 ug/1 40635 1,4-Dichlorobenzene-d4 12.19

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 5-Hexen-2-one 98 C6H10O 000109-49-9 7 2 4-Penten-2-one, 4-methyl- 98 C6H10O 003744-02-3 7 3 2 -Propanone, 1-cyc1opropy1- 98 C6H10O 004160-75-2 5 4 4-Pentan-2-one, 3-methyl-___________ 98 C6H10O 000758-87-2 5 Abundance t Scan 538 (9.968 min): 10159.D (-) m/z 43.00 100.00% 43

5000

58 87 * । ■' 1 1 । ■ 98 9.60 9.80 10.00 10.20 10.40 11"1 r ‘ ‘il - 1III —L ।।" 111" " । 51 ,,, 1 m/ z 58.10 20.41% m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63205:5-Hexen-2-one 43

............ . 5000 960 9.80 10.00 10.20 10.40 55 m/ z 87.05 19.16% 15 27 83 98 I I 38 ,. 50 TVWPmmuman 1 I I >1 I I I I I I I I I I I i I I I I I I I I I I I I I I I I I I I I 1111111 m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #1244: 4-Penten-2-one, 4-methyl- 43 - । । > । 9.60 9.80 10.00 10.20 10.40 5000 m/ z 59.00 11.58% 83 29 55 98 TT-rry ll 30 । । i r i I । i I i I । i i i i | 1 i I I | I I ! | l I I I | I I | I I I I | I I i l J I I I I | I I I I | I T > I | I 1 । । rr । । । > i i | । । I । । i । i । । ।

/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #1306: 2-Propanone, 1 -cyclopropyl- 43 9.60 9.80 10.00 10.20 10.40 m/ z 41.05 A 10.45%

5000

miz-s " " r "1 r " 11 + 29 |!III|I!!I|>'II|II 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 TTTf 69 I I I I I I I I 1 I I I I 83 ponnapoalegoani) 98 111111111.. 1111

9.60 9.80 10.00 10'20 10.40

10159.D GCMS0507.M Thu May 09 11:12:13 2002 Page 2

NYC-WTC_000044812

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GCMS analysis results for unknown compounds, sample AE10165, May 2002 · Box DEP Box 25

NYC-WTC_000044836

Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE10165 on May 10, 2002.

1 shared topics · Same agency, volume and box · similarity 0.999