GCMS analysis results for sample AE11310, May 28, 2002

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Data File : C:\HPCHEM\l\DATA\MAY2102\11309.D Vial: 23 Acq On : 21 May 2002 10:27 pm Operator: Sample : EXTRACTS/14 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0520 .M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 2 5-Hexen-2-one Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 9.91 0.55 ug/1 37220 1,4-Dichlorobenzene-d4 12.14 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 5-Hexe: 2-one 98 C6H10O 000109-49-9 9 2 Aceton 58 C3H60 000067-64-1 7 3 S-(-)/2-Methylbutylamine 87 C5H13N 020626-52-2 7 4 2-Propanone, 1-cyclopropyl-______ 98 C6H10O 004160-75-2 5 Abundance Scan 532 (9.914 min): 11309.D (-) m/ z 43.05 100.00% 43

5000

58 87 ' ' ' 1 1 1 98 9.60 9.80 10.00 10.20

mz-> r ■" i H +9 A— m TPPT 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 69 r " ■ i ‘।1 r1" i m/z 58.10 19.37% Abundance #63205:5-Hexen-2-one 43

5000 ‘ ‘I’ /A 9.60 9.80 10.00 10.20 55 m/z 87.05 16.94% 15 27 I 38 , 50 83 98 I"111''1 ■ ........... i" " r ■" r1" i" " r11' r "11" " r11 r i" " i mz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #94: Acetone 43 9.60 9.80 10.00 10.20 5000 m/ z 59.10 11.58% 15 58 27 - ■ । । । । । । । I I । I । । । । । । । । । I । *t I T I " 1 T ' "I" 1 'I " ' 'I "" I"" I'1" I" 11 I" " I n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #764: S-(-)-2-Methylbutylamine ' ■ । 1 ■ ■ ' i ■ ■ ' ■ । ■ ' ' ■ । 30 9.60 9.80 10.00 10.20 m/z 41.05 11.13% N 5000

41 56 70 87 TT0———TT1T0puammmppr m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 9.60 9.80 10.00 10.20

11309.D GCMS0520.M Wed May 22 09:21:35 2002 Page 2

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