GC/MS calibration table for TCLP analysis, Oct 18 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1801\LB.D Vial: 2 Acq On : 18 Oct 2001 5:09 pm Operator: 209 GTiLOS Sample : lab blk 10/15 Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 6.37 0.47 ug/1 45805 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 B-HexanoXe 100 C6H12O 000589-38-8 90 2 3-Pent^one, 2-methyl- 100 C6H12O 000565-69-5 47 3 3-Bu X-2-ol 72 C4H8O 000598-32-3 38 4 2,4^ 'entanedione 100 C5H8O2 000123-54-6 35 4bundance Scan 145 (6.368 min); LB.D (-) m/z 43.05 100.00% 4t3 57

71 5000 100

600 6.20 6.40 6.60 6.80 rrrrp I J| + I.... . I"'' I m/z 57.00 88.73% ■nZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1528; 3-Hexanone 43 57

29 71 5000 6.00 6.20 6.40 6.60 6.80 100 m/z 71.00 55.02% 85 ft tttt+ ■WprrrrrrTTTT ' I " ’ ' I' I U I Ti/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 ^bundance ,

5000 43 #63399; 3-Pentanone, 2-methyl- 5(7 jkj/k 600 m/z 100.05 6.20 6.40 6.60 31.95% 6.80

A 71 100 85 " I'' . .....I -m- tVz-> Abundance 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105

43 #62480; 3-Buten-2-ol 5f7 .... lys... 6 00 6.20 6.40 6.60 6.80 In/z 41700 25.52%

5000

Tl/Z-> 27 71

20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 I " '' I' " ' I Jul. 6.00 6.20 6.40 6.60 6.80

LB.D NP091101.M Fri Oct 19 10:25:48 2001 Page 1

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