Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
NYC-WTC_000088700–000088724Folder label: “GC/MS Scan 9/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\LB.D Vial: 3 Acq On : 16 Oct 2001 4:11 pm Operator: 209 GALOS Sample : lab blk 9/27 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE ’Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 16 R.T. EstConc Area Relative to ISTD R.T.
6.37 0.46 ug/1 43637 1,4-Dichlorobenzene-d4 11.76
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 3-Hexanone 100 C6H12O 000589-38-8 91 2 Hexaney/3,3,4-trimethyl- 128 C9H20 016747-31-2 45 . 3 Butan^ 2,2-dimethyl- 86 C6H14 000075-83-2 36 4 Hept^^e, 3,3-dimethyl- 128 C9H20 004032-86-4 36. ■ ^bundanceZ- Scan 145 (6.370 min): LB.D (-) m/z 43.00 100.00% 43 5,7 A 71 553 100 600 6.20 6.40 6.60 6.80
m/z-> .................... 10 20 30 40 49 60 n-" 70 . ............. 80 90 L 110 120 100 m/z 5^700 93.04% Abundance #63358; 3-Hexanone 43 57
71 5000 600 6.20 6.40 6:60 6.80 100 m/z 71.00 63.35% 85 ■I"'''''............ 'I Ti/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #5135: Hexane. 3,3,4-trimethyl- 43 57 71
600 6.20 6.40 6.60 6.80 553 m/z 100.05 30.53% A 27 99 JI..................... j" , --113- ; tVz-> Abundance 10 20 30 40 50 60 70 80 #732; Butane, 2,2-dimethyl- ------ 43— 5!7 90 100 110 120 s .'-j-.'.j-j-'-i j '1 ' ' ' ' I ' T"6:ob" 6.20 6.40 6.60 6.80 71 m/ z 41.05 27.39% 29 5000
15 ’ I ' I ' I• ' I ' ' ' ' I I +nr-n-T^ h " " I'l ■nZz-> 10 20 30 40 50 60 70 80 ' 90 100 110 120’ ■ 6.00 6.20 6.40' 6.60 6.80
LB.D NP091101.M Thu Oct 18 10:43:38 2001 Page i
NYC-WTC_000088706
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NYC-WTC_000089278
GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
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Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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GC/MS analysis report with TCLP calibration table data from October 16, 2001.
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Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000086788
Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Laboratory report documenting GC/MS analysis of sample AD23799 conducted on November 1, 2001, identifying unknown compounds.
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Laboratory report documenting GC/MS analysis of sample AD23503 conducted on October 19, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000086624
Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089418
Laboratory report documenting GC/MS analysis of sample AD23836 conducted on November 1, 2001, identifying unknown compounds.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069154
Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
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Gas chromatography-mass spectrometry scan results recorded on September 27, 2001 for environmental samples.
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Fragmented GC/MS scan page from a laboratory blank sample dated September 27, 2001.
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