GC/MS TCLP calibration table analysis, October 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1501\LB.D Vial: 3 Acq On : 15 Oct 2001 1:28 pm Operator: 209 GALOS Sample ; lab blk 9/28 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title ; 209 625/TCLP calibration table 7/16/01 Library : C;\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 8 R.T. EstConc Area Relative to'ISTD R.T.

6.37 0.43 ug/1 47032 1,4-Dichlorobenzene-d4 11.76

Hit# Of 5 Tentative ID MW MolForm CAS# Qua!

1 3-Hexanone 100 C6H12O 000589-38-8 86 2 3-Pent^one, 2-methyl- 100 C6H12O 000565-69-5 58 3 Butan^ 2,2-dimethyl- 86 C6H14 000075-83-2 53 4 Hexai^, 3,3,4- trimethyl - 128 C9H20 _^____O1£74723122 42 Abundance/ Scan 144 (6.365 min): LB.D (-) m/z 43.00 100.00% 43 517 71

5000 100

RFi 600 6.20 6.40 6.60 6.80 51 , I” "I"”I'• " I . ....... .. I-"!'.......I'".......... ""I""!' m/z 57.00 99.10% Ti/z-> Abundance 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 #63358:3-Hexanone 40 1 57

5000 71 6 00 6.20 6.40 6.60 6.80 100 "m/z 71.00 69.46% ...... 85 +-T ■n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63398:3-Pentanone, 2-methyl-

43 6.00 . 6.20 6.40 6.60 6.80 5000- m/z 100.05 37.95% 100 71

iprrT|-irii|l ---- —85------- ..... TlZz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance- #732: Butane, 2,2-dimethyl-—. - ■:6:oo7Y6:2o ;6.40^6.60- 6:80' 71 Wz 41700 28.72% 29 5000

15 I.................. +rpTTTprrTt I'' I" " I" " I" " I" " I'" 'I ""I" " I nZz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 6.00 6.20 6.40 6.60 6.80

LB.D NP091101.M Tue Oct 16 15:20:25 2001 Page 1

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