GC/MS analysis report with TCLP calibration table data from October 16, 2001.
NYC-WTC_000089030–000089044Folder label: “GC/MS Scan 9/28/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1501\LB.D Vial: 3 Acq On : 15 Oct 2001 1:28 pm Operator: 209 GALOS Sample ; lab blk 9/28 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title ; 209 625/TCLP calibration table 7/16/01 Library : C;\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 8 R.T. EstConc Area Relative to'ISTD R.T.
6.37 0.43 ug/1 47032 1,4-Dichlorobenzene-d4 11.76
Hit# Of 5 Tentative ID MW MolForm CAS# Qua!
1 3-Hexanone 100 C6H12O 000589-38-8 86 2 3-Pent^one, 2-methyl- 100 C6H12O 000565-69-5 58 3 Butan^ 2,2-dimethyl- 86 C6H14 000075-83-2 53 4 Hexai^, 3,3,4- trimethyl - 128 C9H20 _^____O1£74723122 42 Abundance/ Scan 144 (6.365 min): LB.D (-) m/z 43.00 100.00% 43 517 71
5000 100
RFi 600 6.20 6.40 6.60 6.80 51 , I” "I"”I'• " I . ....... .. I-"!'.......I'".......... ""I""!' m/z 57.00 99.10% Ti/z-> Abundance 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 #63358:3-Hexanone 40 1 57
5000 71 6 00 6.20 6.40 6.60 6.80 100 "m/z 71.00 69.46% ...... 85 +-T ■n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63398:3-Pentanone, 2-methyl-
43 6.00 . 6.20 6.40 6.60 6.80 5000- m/z 100.05 37.95% 100 71
iprrT|-irii|l ---- —85------- ..... TlZz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance- #732: Butane, 2,2-dimethyl-—. - ■:6:oo7Y6:2o ;6.40^6.60- 6:80' 71 Wz 41700 28.72% 29 5000
15 I.................. +rpTTTprrTt I'' I" " I" " I" " I" " I'" 'I ""I" " I nZz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 6.00 6.20 6.40 6.60 6.80
LB.D NP091101.M Tue Oct 16 15:20:25 2001 Page 1
NYC-WTC_000089036
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NYC-WTC_000088491
Calibration data table for TCLP analysis using GC/MS standards processed on October 18, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088700
Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088184
Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089278
GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000086624
Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000086788
Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000087496
Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067739
Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 25, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068559
Calibration data table for GC/MS instrument used in TCLP analysis, generated on November 5, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067428
Laboratory report detailing GCMS analysis of sample AD22558 conducted on October 1, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068400
Multi-page laboratory log table recording sample extraction details including volumes and drip rates for GCMS analysis in November 2001.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067979
Calibration data table for GCMS TCLP analysis listing surrogate compounds and response factors from November 2, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000089025
Fragmented GC/MS scan page from a laboratory blank sample dated September 28, 2001.
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NYC-WTC_000089026
Fragmented GC/MS scan page from a laboratory blank sample dated September 28, 2001.
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NYC-WTC_000089045
Laboratory report documenting GC/MS analysis of sample AD23652 conducted on October 16, 2001.
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NYC-WTC_000089059
Laboratory report documenting GC/MS analysis of sample AD23651 conducted on October 16, 2001.
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NYC-WTC_000089073
Laboratory record for sample AD23653 showing detection of unknown compounds on October 16, 2001.
Filed in the same folder